N-methyl-dec-9-ynanilide

Base Information

• Chemical Name: N-methyl-dec-9-ynanilide
• CAS No.: 109734-34-1
• Molecular Formula: C₁₇H₂₃NO
• Molecular Weight: 257.376
• Mol file: 109734-34-1.mol

Synonyms:N-methyl-dec-9-ynanilide

Chemical Property of N-methyl-dec-9-ynanilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-methyl-dec-9-ynanilide

There total 2 articles about N-methyl-dec-9-ynanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dec-9-ynoic acid (1642-49-5) → N-methyl-dec-9-ynanilide (109734-34-1)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: benzene; pyridine

With pyridine; thionyl chloride; benzene;

DOI:10.1111/j.1945-5100.2002.tb01105.x

Reference yield:

9-decynoic acid chloride (100131-19-9) + N-methylaniline (100-61-8) → N-methyl-dec-9-ynanilide (109734-34-1)

Guidance literature:

With pyridine; benzene;

DOI:10.1111/j.1945-5100.2002.tb01105.x

Reference yield:

N-methyl-dec-9-ynanilide (109734-34-1) → 2-n-nonyl-1,3-dioxolane (4353-06-4)

Guidance literature:

Multi-step reaction with 3 steps

1: lithium alanate; diethyl ether

2: benzene; sulfuric acid / Unter Entfernen des entstehenden Wassers

3: platinum; ethyl acetate / Hydrogenation

With lithium aluminium tetrahydride; diethyl ether; sulfuric acid; ethyl acetate; platinum; benzene;

DOI:10.1111/j.1945-5100.2002.tb01105.x

upstream raw materials:

9-decynoic acid chloride

N-methylaniline

dec-9-ynoic acid

Downstream raw materials:

2-n-nonyl-1,3-dioxolane