Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester

Base Information

Chemical Name:Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester
CAS No.:101836-61-7
Molecular Formula:C₁₇H₂₀O₅
Molecular Weight:304.343
Hs Code.:

Synonyms:Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester

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Chemical Property of Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester

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Technology Process of Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester

There total 6 articles about Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 285-67-6
Cyclopentene oxide

: 101836-61-7
Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / sulfuric acid / 1 h / 95 °C

2: 1.) oxalyl chloride, DMSO; 2.) triethylamine / 1.) CH₂Cl₂, -78 deg C, 15 min; 2.) CH₂Cl₂, warming to r.t. 1 h

3: 100 percent / MgSO₄ / diethyl ether / 48 h

4: 95 percent / triethylamine / benzene / 6 h / Heating

5: 10.62 g / glacial acetic acid, water / tetrahydrofuran / 18 h / Ambient temperature

With oxalyl dichloride; sulfuric acid; water; magnesium sulfate; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/ja00271a038

Reference yield:

: 101836-57-1
2-(benzyloxy)cyclopentanol

: 101836-61-7
Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) oxalyl chloride, DMSO; 2.) triethylamine / 1.) CH₂Cl₂, -78 deg C, 15 min; 2.) CH₂Cl₂, warming to r.t. 1 h

2: 100 percent / MgSO₄ / diethyl ether / 48 h

3: 95 percent / triethylamine / benzene / 6 h / Heating

4: 10.62 g / glacial acetic acid, water / tetrahydrofuran / 18 h / Ambient temperature

With oxalyl dichloride; water; magnesium sulfate; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/ja00271a038

Reference yield:

: 101836-58-2
α-benzyloxycyclopentanone

: 101836-61-7
Acetic acid 2-(3-benzyloxy-2-oxo-cyclopentyl)-1-methyl-2-oxo-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / MgSO₄ / diethyl ether / 48 h

2: 95 percent / triethylamine / benzene / 6 h / Heating

3: 10.62 g / glacial acetic acid, water / tetrahydrofuran / 18 h / Ambient temperature

With water; magnesium sulfate; acetic acid; triethylamine; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/ja00271a038