Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester

Base Information

Chemical Name:Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester
CAS No.:101836-60-6
Molecular Formula:C₂₁H₂₇NO₅
Molecular Weight:373.449
Hs Code.:

Synonyms:Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester

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Technology Process of Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester

There total 5 articles about Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 38939-83-2
2-acetoxypropionyl chloride

: 101836-59-3
4-(5-Benzyloxy-cyclopent-1-enyl)-morpholine

: 101836-60-6
Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester

Guidance literature:: With triethylamine; In benzene; for 6h; Heating;
DOI:10.1021/ja00271a038

Reference yield:

: 285-67-6
Cyclopentene oxide

: 101836-60-6
Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / sulfuric acid / 1 h / 95 °C

2: 1.) oxalyl chloride, DMSO; 2.) triethylamine / 1.) CH₂Cl₂, -78 deg C, 15 min; 2.) CH₂Cl₂, warming to r.t. 1 h

3: 100 percent / MgSO₄ / diethyl ether / 48 h

4: 95 percent / triethylamine / benzene / 6 h / Heating

With oxalyl dichloride; sulfuric acid; magnesium sulfate; dimethyl sulfoxide; triethylamine; In diethyl ether; benzene;
DOI:10.1021/ja00271a038

Reference yield:

: 101836-57-1
2-(benzyloxy)cyclopentanol

: 101836-60-6
Acetic acid 2-(3-benzyloxy-2-morpholin-4-yl-cyclopent-1-enyl)-1-methyl-2-oxo-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) oxalyl chloride, DMSO; 2.) triethylamine / 1.) CH₂Cl₂, -78 deg C, 15 min; 2.) CH₂Cl₂, warming to r.t. 1 h

2: 100 percent / MgSO₄ / diethyl ether / 48 h

3: 95 percent / triethylamine / benzene / 6 h / Heating

With oxalyl dichloride; magnesium sulfate; dimethyl sulfoxide; triethylamine; In diethyl ether; benzene;
DOI:10.1021/ja00271a038