[(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate

Base Information

Chemical Name:[(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate
CAS No.:223424-81-5
Molecular Formula:BF₄*C₂₀H₂₈MnP₂
Molecular Weight:472.132
Hs Code.:

Synonyms:[(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate

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Chemical Property of [(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate

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Technology Process of [(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate

There total 2 articles about [(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1282-37-7
ferrocenium(III) tetrafluoroborate

: 223424-72-4
(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(II)

: 223424-81-5
[(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate

Guidance literature:: In dichloromethane; N2-atmosphere; stirring (-50°C, 3 h), pptn. on Et2O addn.; repptn. (CH2Cl2 / Et2O), washing (Et2O), evapn.; elem. anal.;
DOI:10.1021/om9810549

Reference yield: 85.0%

: 1282-37-7
ferrocenium(III) tetrafluoroborate

: 223424-74-6
(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

: 223424-81-5
[(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate

Guidance literature:: In dichloromethane; N2-atmosphere; stirring (-30°C, 2 h), pptn. on Et2O addn.; collecting, repptn., washing (Et2O), evapn.;
DOI:10.1021/om9810549

Reference yield: 89.0%

: 223424-81-5
[(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(III)] tetrafluoroborate

: 223424-72-4
(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(II)

Guidance literature:: With (MeC₅H₄)2Co; In dichloromethane; N2-atmosphere; stirring (-50°C, 3 h), evapn.; extg. (pentane), filtering, concg., crystn. (-80°C);
DOI:10.1021/om9810549