(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

Base Information

Chemical Name:(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)
CAS No.:223424-74-6
Molecular Formula:C₂₀H₂₉MnP₂
Molecular Weight:386.336
Hs Code.:

Synonyms:(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

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Chemical Property of (1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

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Technology Process of (1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

There total 6 articles about (1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 74507-62-3
bis(pentamethylcyclopentadienyl)cobalt(II)

: [Mn(η5-methylcyclopentadienyl)(bis(1,2-dimethylphosphino)ethane)(CC(H)Ph)]2[PF6]2

: 223424-74-6
(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

Guidance literature:: In not given;
DOI:10.1021/om034237q

Reference yield: 98.0%

: [(η5-methylcyclopentadienyl)Mn(1,2-bis(dimethylphosphino)ethane)(CC(Ph)SnMe3)]

: 223424-74-6
(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

Guidance literature:: With methanol; In toluene; (N2); using Schlenk techniques; addn. of excess MeOH to toluene soln. of((C5H4Me)Mn(dmpe)CC(Ph)SnMe3); stirring at room temp. for 2 h; removal of solvent under vac., extn. with pentane,, filtration, evapn. of pentane fraction, crystn. from pentane at -35°C; elem. anal.;
DOI:10.1021/om049284c

Reference yield: 87.0%

: [HMo(CO)3(η5-pentamethylcyclopentadienyl)]

: 223424-72-4
(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylethynyl)manganese(II)

: di[(pentamethylcyclopentadienyl)molybdenum]hexacarbonyl

: 223424-74-6
(1,2-bis(dimethylphosphino)ethane)(η(5)-methylcyclopentadienyl)(phenylvinylidene)manganese(I)

Guidance literature:: In benzene; N2-atmosphere; stirring (15 min), evapn. (reduced pressure); extg. (pentane), filtering, concg., crystn. (-35°C);
DOI:10.1021/om9810549