4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al

Base Information

Chemical Name:4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al
CAS No.:223691-84-7
Molecular Formula:C₁₄H₁₈O₂
Molecular Weight:218.296
Hs Code.:

Synonyms:4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al

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Chemical Property of 4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al

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Technology Process of 4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al

There total 27 articles about 4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 401895-10-1
4-(4-methoxy-phenyl)-4-methyl-hex-5-en-1-ol

: 223691-84-7
4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1081/SCC-200063941

Reference yield: 87.0%

: 223691-80-3
1-methoxy-4-(4-methoxyphenyl)-4-methylhexa-1,5-diene

: 223691-84-7
4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 1.5h;
DOI:10.1081/SCC-200061679

Reference yield:

: 1712-69-2
1-isopropenyl-4-methoxybenzene

: 223691-84-7
4-(4-methoxyphenyl)-4-methyl-hex-5-en-1-al

Guidance literature:: Multi-step reaction with 7 steps

1.1: Zn-Cu / diethyl ether / 25 °C

2.1: Zn; NH₄Cl / methanol

3.1: 84 percent / methanol

4.1: 74 percent / BuLi / tetrahydrofuran / -78 - 70 °C

5.1: 4,5-dihydroimidazol-2-ylidene-Ru / toluene / 48 h / 80 °C

6.1: 9-BBN / tetrahydrofuran / 25 °C

6.2: 50 percent / H₂O₂; aq. NaOH

7.1: 77 percent / Dess-Martin periodinane

With 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; copper; ammonium chloride; Dess-Martin periodane; zinc; 4,5-dihydroimidazol-2-ylidene-Ru; In tetrahydrofuran; methanol; diethyl ether; toluene; 3.1: Shapiro reaction;
DOI:10.1016/S0040-4039(01)02007-X