C₄₅H₃₉ClFN₅O₅

Base Information

Chemical Name:C₄₅H₃₉ClFN₅O₅
CAS No.:1615696-49-5
Molecular Formula:C₄₅H₃₉ClFN₅O₅
Molecular Weight:784.287
Hs Code.:

C<sub>45</sub>H<sub>39</sub>ClFN<sub>5</sub>O<sub>5</sub>

Synonyms:C₄₅H₃₉ClFN₅O₅

Suppliers and Price of C₄₅H₃₉ClFN₅O₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₅H₃₉ClFN₅O₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₅H₃₉ClFN₅O₅

There total 6 articles about C₄₅H₃₉ClFN₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.5%

: 1615696-48-4
C₂₅H₂₃ClFN₅O₄

: 14470-28-1
mono-4-methoxytrityl chloride

: 1615696-49-5
C₄₅H₃₉ClFN₅O₅

Guidance literature:: With 2,3,5-trimethyl-pyridine; silver nitrate; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 1615696-39-3
C₂₁H₂₃FO₅

: 1615696-49-5
C₄₅H₃₉ClFN₅O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / acetic acid / 12 h / 0 - 20 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 4 h / 0 - 60 °C

3.1: silver nitrate; 2,3,5-trimethyl-pyridine / dichloromethane / 12 h / 20 °C

With 2,3,5-trimethyl-pyridine; sulfuric acid; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetic acid; acetonitrile;

Reference yield:

: methyl 5-O-benzyl-3-deoxy-3-fluoro-α-D-ribofuranoside

: 1615696-49-5
C₄₅H₃₉ClFN₅O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 12 h / 80 °C

2.1: tetrahydrofuran / 12 h / -78 - 20 °C / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Cooling with ice

4.1: sulfuric acid / acetic acid / 12 h / 0 - 20 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / 0 - 20 °C / Inert atmosphere

5.2: 4 h / 0 - 60 °C

6.1: silver nitrate; 2,3,5-trimethyl-pyridine / dichloromethane / 12 h / 20 °C

With 2,3,5-trimethyl-pyridine; dmap; sulfuric acid; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; acetic acid; acetonitrile;