lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>-phenoxysilicate (1-)

Base Information

• Chemical Name: lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>-phenoxysilicate (1-)
• CAS No.: 97878-09-6
• Molecular Formula: C₂₄H₁₃F₁₂O₃Si*Li
• Molecular Weight: 612.373

Synonyms:lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>-phenoxysilicate (1-)

Chemical Property of lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>-phenoxysilicate (1-)

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Technology Process of lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>-phenoxysilicate (1-)

There total 7 articles about lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>-phenoxysilicate (1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tetramethylammonium Bis<α,α-bis(trifluoromethyl)-benzenemethanolato(2-)-C2,O>phenylsilicate (70083-69-1) → lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>-phenoxysilicate (1-) (97878-09-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / Br₂ / 24 h / 25 °C

2: 4.78 g / n-BuLi / tetrahydrofuran / 1.) 0 deg C, 30 min.; 2.) 25 deg C, 1 h

With n-butyllithium; bromine; In tetrahydrofuran;

DOI:10.1021/ja00308a030

Reference yield:

(TB-5-11)-bis-(1,1,1,3,3,3-hexafluoro-2-phenyl-propan-2-olato(2-)-C2',O)-phenyl-silicate(1-); lithium salt (70083-67-9) → lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>-phenoxysilicate (1-) (97878-09-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 59.6 percent / CH₂Cl₂

2: 72 percent / Br₂ / 24 h / 25 °C

3: 4.78 g / n-BuLi / tetrahydrofuran / 1.) 0 deg C, 30 min.; 2.) 25 deg C, 1 h

With n-butyllithium; bromine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00308a030

Reference yield:

tetraethylammonium bis<α,α-bis(trifluorometyl)benzenemethanolato(2-)-C2,O>-n-butylsilicate(1-) (97878-04-1) → lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>-phenoxysilicate (1-) (97878-09-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 74.6 percent / Br₂ / 24 h / 25 °C

2: 4.78 g / n-BuLi / tetrahydrofuran / 1.) 0 deg C, 30 min.; 2.) 25 deg C, 1 h

With n-butyllithium; bromine; In tetrahydrofuran;

DOI:10.1021/ja00308a030

upstream raw materials:

C₁₈H₈F₁₂O₂Si

phenol

(TB-5-11)-bis-(1,1,1,3,3,3-hexafluoro-2-phenyl-propan-2-olato^(2-)-C^2',O)-phenyl-silicate^(1-); lithium salt

Tetramethylammonium Bis<α,α-bis(trifluoromethyl)-benzenemethanolato(2-)-C²,O>phenylsilicate

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