7-(2,6-difluoro-phenyl)-1λ⁴,3λ⁴,5λ⁴-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene

Base Information

• Chemical Name: 7-(2,6-difluoro-phenyl)-1λ⁴,3λ⁴,5λ⁴-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene
• CAS No.: 662141-73-3
• Molecular Formula: C₇H₃F₂N₅S₃
• Molecular Weight: 291.329

Synonyms:7-(2,6-difluoro-phenyl)-1λ⁴,3λ⁴,5λ⁴-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene

Chemical Property of 7-(2,6-difluoro-phenyl)-1λ⁴,3λ⁴,5λ⁴-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene

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Technology Process of 7-(2,6-difluoro-phenyl)-1λ⁴,3λ⁴,5λ⁴-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene

There total 1 articles about 7-(2,6-difluoro-phenyl)-1λ⁴,3λ⁴,5λ⁴-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

C16H30F2N2Si3 → 7-(2,6-difluoro-phenyl)-1λ4,3λ4,5λ4-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene (662141-73-3)

Guidance literature:

With trithiazyl trichloride; In acetonitrile;

DOI:10.1002/ejic.200300111

Reference yield: 65.0%

Hexafluorobenzene (392-56-3) + 7-(2,6-difluoro-phenyl)-1λ4,3λ4,5λ4-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene (662141-73-3) → 7-(2,6-difluoro-phenyl)-1λ4,3λ4,5λ4-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene; compound with 1,2,3,4,5,6-hexafluoro-benzene

Guidance literature:

With hexane; at 20 ℃; for 48h;

DOI:10.1002/ejic.200300951

Reference yield:

7-(2,6-difluoro-phenyl)-1λ4,3λ4,5λ4-trithia-2,4,6,8,9-pentaaza-bicyclo[3.3.1]nona-1(8),2,3,5(9),6-pentaene (662141-73-3) → C7H3F2N2S2

Guidance literature:

Thermolysis;

DOI:10.1016/j.mencom.2007.06.005

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