3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil

Base Information

Chemical Name:3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil
CAS No.:809290-41-3
Molecular Formula:C₂₈H₄₂N₂O₈Si₂
Molecular Weight:590.821
Hs Code.:

Synonyms:3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil

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Chemical Property of 3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil

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Technology Process of 3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil

There total 2 articles about 3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 98-88-4
benzoyl chloride

: 104477-70-5
5',3'-O-(tetraisopropyldisiloxane-1,3-di-yl)-1-β-D-arabinofuranosyl-uracil

: 809290-41-3
3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil

Guidance literature:: 5',3'-O-(tetraisopropyldisiloxane-1,3-di-yl)-1-β-D-arabinofuranosyl-uracil; With chloro-trimethyl-silane; triethylamine; In dichloromethane; at 20 ℃; for 2h;

benzoyl chloride; With pyridine; N-ethyl-N,N-diisopropylamine; at 20 ℃; for 17h;

With toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; for 0.166667h;
DOI:10.1016/j.tet.2004.09.023

Reference yield: 34.0%

: 98-88-4
benzoyl chloride

: 104477-70-5
5',3'-O-(tetraisopropyldisiloxane-1,3-di-yl)-1-β-D-arabinofuranosyl-uracil

: 809290-41-3
3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil

: Benzoic acid (2R,3S,3aR,9aR)-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl ester

Guidance literature:: With tetrabutylammomium bromide; sodium carbonate; In dichloromethane; water;
DOI:10.1016/j.tet.2004.09.023

Reference yield: 92.0%

: 809290-41-3
3-N-benzoyl-1-(3',5'-O,O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl)uracil

: 1469-70-1
allyl ethyl carbonate

: 1-((2R,3S,3aR,9aR)-3-Allyloxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-3-benzoyl-1H-pyrimidine-2,4-dione

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,4-di(diphenylphosphino)-butane; In tetrahydrofuran; for 3h; Heating;
DOI:10.1016/j.tet.2004.09.023