(-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane

Base Information

Chemical Name:(-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane
CAS No.:929217-69-6
Molecular Formula:C₂₂H₂₃F₃O₄
Molecular Weight:408.417
Hs Code.:

Synonyms:(-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane

There total 1 articles about (-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 929217-58-3
(-)-[(4R,5R)-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-hydroxy-1-phenylethyl)-[1,3]dioxolan-4-yl]phenylmethanone

: 74-88-4
methyl iodide

: 929217-69-6
(-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane

Guidance literature:: With potassium tert-butylate; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1021/jo062016z

Reference yield: 88.0%

: 929217-69-6
(-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane

: (+)-(1S,3S,4R)-5,5,5-trifluoro-3-hydroxy-1,4-dimethoxy-1,4-diphenylpentan-2-one

Guidance literature:: With methanol; acetyl chloride; for 3h; Heating;
DOI:10.1021/jo062016z

Reference yield:

: 929217-69-6
(-)-(R)-4-[1-methoxy-1-phenylmeth-(E)-ylidene]-2,2-dimethyl-5-((R)-2,2,2-trifluoro-1-methoxy-1-phenylethyl)-[1,3]dioxolane

: 26164-26-1
(S)-2-methoxy-2-phenylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / AcCl; MeOH / 3 h / Heating

2: H₅IO₆ / diethyl ether / 0 - 20 °C

With methanol; periodic acid; acetyl chloride; In diethyl ether;
DOI:10.1021/jo062016z