(S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid

Base Information

• Chemical Name: (S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid
• CAS No.: 1354752-75-2
• Molecular Formula: C₂₁H₁₉NO₅
• Molecular Weight: 365.386

Synonyms:(S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid

Chemical Property of (S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

(S)-Fmoc-2-amino-3-propargyloxy-propionicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of (S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid

There total 7 articles about (S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

O-propargyl-L-serine hydrochloride (1379150-93-2) + sodium carbonate (497-19-8) + N-(Fluoren-9-ylmethoxy)succimimide → (S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid (1354752-75-2)

Guidance literature:

In 1,4-dioxane; water; at 0 ℃; for 3h;

DOI:10.1039/c7cc07859e

Reference yield: 97.0%

N-[((9H-fluoren-9-yl)methoxy)carbonyl]-O-(prop-2-yn-1-yl)serine methyl ester → (S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid (1354752-75-2)

Guidance literature:

With calcium chloride; lithium hydroxide; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c7ob01388d

Reference yield: 90.0%

C6H9NO3*C2HF3O2 + N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide (82911-69-1) → (S)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-3-(prop-2-yn-1-yloxy)propanoic acid (1354752-75-2)

Guidance literature:

With sodium carbonate; In water; acetone;

upstream raw materials:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

(S)-2-[(tert-butoxycarbonyl)amino]-3-(prop-2-yn-1-yloxy)propanoic acid

O-propargyl-L-serine hydrochloride

N-[(1,1-dimethylethoxy)carbonyl]-O-(prop-2-yn-1-yl)serine methyl ester

Downstream raw materials:

C₃₈H₅₅N₁₁O₁₁

C₃₂H₄₄N₈O₆

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