1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide

Base Information

Chemical Name:1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide
CAS No.:866819-61-6
Molecular Formula:C₁₆H₁₆ClN₃OS
Molecular Weight:333.842
Hs Code.:

Synonyms:1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide

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Chemical Property of 1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide

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Technology Process of 1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide

There total 4 articles about 1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 536-40-3
4-chlorobenzoic acid hydrazide

: 19241-16-8
2,6-dimethylphenylisothiocyanate

: 866819-61-6
1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide

Guidance literature:: In methanol; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2010.08.034

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 866819-61-6
1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / methanol / Reflux

2: methanol / Reflux

With ammonia; In methanol;
DOI:10.1071/CH12134

Reference yield:

: 1126-46-1
Methyl 4-chlorobenzoate

: 866819-61-6
1-[(4′-chlorophenyl)carbonyl-4-(2″,6″-dimethylphenyl)]thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / Reflux

2: methanol / Reflux

With hydrazine hydrate; In methanol;
DOI:10.1071/CH12134