3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Base Information

Chemical Name:3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide
CAS No.:1377616-51-7
Molecular Formula:C₁₈H₂₀N₄O₃S₂
Molecular Weight:404.514
Hs Code.:

Synonyms:3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

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Chemical Property of 3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Chemical Property:

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Technology Process of 3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

There total 10 articles about 3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(5-carbamoyl-2-isopropoxy-phenylamino)-4'-methyl-[4,5']bithiazolyl-2'-carboxylic acid ethyl ester hydrobromide

: 1377616-51-7
3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Guidance literature:: With sodium tetrahydroborate; ethanol; at 70 ℃; for 4h;

Reference yield:

: 1694-29-7
3-chloropentane-2,4-dione

: 1377616-51-7
3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 2 h / 100 °C

2: bromine / 1,4-dioxane / 6 h / 50 °C

3: ethanol / 24 h / 20 °C

4: ethanol; sodium tetrahydroborate / 4 h / 70 °C

With sodium tetrahydroborate; ethanol; bromine; In 1,4-dioxane; ethanol;

Reference yield:

: 1369838-81-2
4-Isopropoxy-3-nitro-benzamide

: 1377616-51-7
3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate; methanol; nickel(II) chloride hexahydrate / 1 h / 0 - 23 °C

2: sodium hydrogencarbonate / chloroform; water / 3.17 h / 20 °C

3: ammonia / methanol / 16 h / 20 °C

4: ethanol / 24 h / 20 °C

5: ethanol; sodium tetrahydroborate / 4 h / 70 °C

With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate; ethanol; ammonia; sodium hydrogencarbonate; In methanol; ethanol; chloroform; water;