3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Base Information

Chemical Name:3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide
CAS No.:1377581-81-1
Molecular Formula:C₁₈H₁₉ClN₄O₂S₂
Molecular Weight:422.959
Hs Code.:

Synonyms:3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

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Chemical Property of 3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Chemical Property:

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Technology Process of 3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

There total 10 articles about 3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1377616-51-7
3-(2'-hydroxymethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

: 1377581-81-1
3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; for 6h;

Reference yield:

: 1694-29-7
3-chloropentane-2,4-dione

: 1377581-81-1
3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol / 2 h / 100 °C

2: bromine / 1,4-dioxane / 6 h / 50 °C

3: ethanol / 24 h / 20 °C

4: ethanol; sodium tetrahydroborate / 4 h / 70 °C

5: triethylamine; methanesulfonyl chloride / dichloromethane / 6 h

With sodium tetrahydroborate; ethanol; bromine; methanesulfonyl chloride; triethylamine; In 1,4-dioxane; ethanol; dichloromethane;

Reference yield:

: 1377581-87-7
4-Isopropoxy-3-isothiocyanato-benzamide

: 1377581-81-1
3-(2'-chloromethyl-4'-methyl-[4,5']bithiazolyl-2-ylamino)-4-isopropoxy-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / methanol / 16 h / 20 °C

2: ethanol / 24 h / 20 °C

3: ethanol; sodium tetrahydroborate / 4 h / 70 °C

4: triethylamine; methanesulfonyl chloride / dichloromethane / 6 h

With sodium tetrahydroborate; ethanol; ammonia; methanesulfonyl chloride; triethylamine; In methanol; ethanol; dichloromethane;