ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

Base Information

Chemical Name:ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate
CAS No.:123753-53-7
Molecular Formula:C₁₅H₁₆N₆O₄
Molecular Weight:344.33
Hs Code.:

Synonyms:ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

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Technology Process of ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

There total 1 articles about ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 109182-40-3
ethyl (6-amino-4-hydrazino-5-nitropyridin-2-yl)carbamate

: 100-52-7
benzaldehyde

: 123753-53-7
ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

Guidance literature:: In N,N-dimethyl acetamide; for 17h; Ambient temperature;
DOI:10.1021/jm00164a030

Reference yield: 83.0%

: 123753-53-7
ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

: 123753-54-8
ethyl N-<5,6-diamino-4-(2-benzylidenehydrazino)-pyridin-2-yl>carbamate

Guidance literature:: With hydrogen; nickel; In N,N-dimethyl acetamide; for 1.83333h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00164a030

Reference yield:

: 123753-53-7
ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

: 123753-55-9
ethyl N-<4-amino-1-(2-benzylideneamino)imidazo<4,5-c>pyridin-6-yl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / H₂ / Raney nickel / N,N-dimethyl-acetamide / 1.83 h / 760 Torr / Ambient temperature

2: 36 percent / Et₃N / N,N-dimethyl-acetamide / 23 h / Ambient temperature

3: 466 mg / Raney nickel / ethanol / 2.5 h / Heating

With hydrogen; nickel; triethylamine; nickel; In ethanol; N,N-dimethyl acetamide;
DOI:10.1021/jm00164a030