methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate

Base Information

Chemical Name:methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate
CAS No.:306990-41-0
Molecular Formula:C₁₉H₁₉ClN₄OS
Molecular Weight:386.905
Hs Code.:

Synonyms:methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate

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Chemical Property of methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate

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Technology Process of methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate

There total 3 articles about methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2740-81-0
2-chlorophenylisothiocyanate

: 161607-20-1
3-(benzotriazol-1-yl)-3-ethoxy-1-propene

: 74-88-4
methyl iodide

: 306990-41-0
methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate

Guidance literature:: 3-(benzotriazol-1-yl)-3-ethoxy-1-propene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

2-chlorophenylisothiocyanate; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jo001159x

Reference yield:

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 306990-41-0
methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hexane / 18 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.2: tetrahydrofuran; hexane / 0.5 h / -78 °C

2.3: 75 percent / tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/jo001159x

Reference yield:

: 3054-95-3
acrylaldehyde diethyl acetal

: 306990-41-0
methyl 2-(1H-1,2,3-benzotriazol-1-yl)-N-(2-chlorophenyl)-2-ethoxy-3-butenimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hexane / 18 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.2: tetrahydrofuran; hexane / 0.5 h / -78 °C

2.3: 75 percent / tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/jo001159x