11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

Base Information

Chemical Name:11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane
CAS No.:66977-69-3
Molecular Formula:C₃₈H₄₈N₄O₆S₃
Molecular Weight:753.02
Hs Code.:

Synonyms:11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

Suppliers and Price of 11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

There total 2 articles about 11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16695-22-0
N,N-bis(tosyloxyethyl)-p-toluenesulfonamide

: N,N'-bis(4-methylbenzenesulfonyl)bis(3-aminopropyl)benzylamine hydrochloride

: 66977-69-3
11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

Guidance literature:: With sodium hydride; Multistep reaction; 1.) DMF, 60 deg C, 2.) DMF, 100-110 deg C;
DOI:10.1021/jm00002a019

Reference yield:

: 66977-69-3
11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

Guidance literature:: Na-Salz des Hydrochlorids (2), N,O,O'-Tritosyldiethanolamin;
DOI:10.1039/c39780000014

Reference yield:

: 66977-69-3
11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

: AMD 6038

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / Pd(OH)2/C / Heating

2: K₂CO₂ / acetonitrile / Heating

3: conc. H₂SO₄ / 100 °C

With formic acid; sulfuric acid; potassium carbonate; palladium dihydroxide; In acetonitrile;
DOI:10.1021/jm00002a019