1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

Base Information

Chemical Name:1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane
CAS No.:1025937-07-8
Molecular Formula:C₇₀H₉₀N₈O₁₂S₆
Molecular Weight:1427.93
Hs Code.:

1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

Synonyms:1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

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Chemical Property of 1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

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Technology Process of 1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

There total 5 articles about 1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66977-69-3
11-benzyl-1,4,7-tris-(toluene-4-sulfonyl)-1,4,7,11-tetraaza-cyclotetradecane

: 1025937-07-8
1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / Pd(OH)2/C / Heating

2: K₂CO₃ / acetonitrile / 50 °C

3: K₂CO₃ / acetonitrile / 60 °C

With formic acid; potassium carbonate; palladium dihydroxide; In acetonitrile;
DOI:10.1021/jm00002a019

Reference yield:

: 16695-22-0
N,N-bis(tosyloxyethyl)-p-toluenesulfonamide

: 1025937-07-8
1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 60 deg C, 2.) DMF, 100-110 deg C

2: formic acid / Pd(OH)2/C / Heating

3: K₂CO₃ / acetonitrile / 50 °C

4: K₂CO₃ / acetonitrile / 60 °C

With formic acid; sodium hydride; potassium carbonate; palladium dihydroxide; In acetonitrile;
DOI:10.1021/jm00002a019

Reference yield:

: N,N'-bis(4-methylbenzenesulfonyl)bis(3-aminopropyl)benzylamine hydrochloride

: 1025937-07-8
1,4,7-Tris-(toluene-4-sulfonyl)-11-{3-[4,8,11-tris-(toluene-4-sulfonyl)-1,4,8,11-tetraaza-cyclotetradec-1-ylmethyl]-benzyl}-1,4,7,11-tetraaza-cyclotetradecane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 60 deg C, 2.) DMF, 100-110 deg C

2: formic acid / Pd(OH)2/C / Heating

3: K₂CO₃ / acetonitrile / 50 °C

4: K₂CO₃ / acetonitrile / 60 °C

With formic acid; sodium hydride; potassium carbonate; palladium dihydroxide; In acetonitrile;
DOI:10.1021/jm00002a019