4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

Base Information

Chemical Name:4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl
CAS No.:443926-31-6
Molecular Formula:C₄₃H₃₈N₂O₂
Molecular Weight:614.787
Hs Code.:

Synonyms:4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

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Chemical Property of 4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

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Technology Process of 4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

There total 5 articles about 4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.2%

: 79-41-4,25087-26-7,50867-57-7
poly(methacrylic acid)

: 194354-29-5
4-[N-(4-hydroxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

: 443926-31-6
4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 10h;
DOI:10.1039/b110088m

Reference yield:

: 624-31-7
4-tolyl iodide

: 443926-31-6
4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / K₂CO₃; copper; 18-crown-6 / 1,2-dichloro-benzene / 14 h / 190 °C

2: 57.8 percent / POCl₃ / 1,2-dichloro-ethane / 5 h / 60 °C

3: 99.7 percent / NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

4: 77.2 percent / DMAP; DCC / tetrahydrofuran / 10 h / 20 °C

With dmap; sodium tetrahydroborate; 18-crown-6 ether; copper; potassium carbonate; dicyclohexyl-carbodiimide; trichlorophosphate; In tetrahydrofuran; water; 1,2-dichloro-ethane; 1,2-dichloro-benzene; 1: Ullmann condensation / 2: Vilsmeier reacton;
DOI:10.1039/b110088m

Reference yield:

: 531-91-9
N,N'-diphenyl-p-phenylenediamine

: 443926-31-6
4-[N-(4-methacryloyloxymethylphenyl)-N-(4-methylphenyl)amino]-4'[N-phenyl-N-(4-methylphenyl)amino]biphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / K₂CO₃; copper; 18-crown-6 / 1,2-dichloro-benzene / 14 h / 190 °C

2: 57.8 percent / POCl₃ / 1,2-dichloro-ethane / 5 h / 60 °C

3: 99.7 percent / NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

4: 77.2 percent / DMAP; DCC / tetrahydrofuran / 10 h / 20 °C

With dmap; sodium tetrahydroborate; 18-crown-6 ether; copper; potassium carbonate; dicyclohexyl-carbodiimide; trichlorophosphate; In tetrahydrofuran; water; 1,2-dichloro-ethane; 1,2-dichloro-benzene; 1: Ullmann condensation / 2: Vilsmeier reacton;
DOI:10.1039/b110088m