5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

Base Information

Chemical Name:5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane
CAS No.:1427184-26-6
Molecular Formula:C₃₂H₄₂O₄Si
Molecular Weight:518.769
Hs Code.:

Synonyms:5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

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Chemical Property of 5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

Chemical Property:

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Technology Process of 5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

There total 4 articles about 5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 172644-48-3
diethyl 2-(2-benzyloxyethyl)-2-hydroxymethylmalonate

: 1427184-26-6
5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / Reflux

2: acetone / 25 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 22 h / 25 °C

With 1H-imidazole; sodium tetrahydroborate; In methanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1462-37-9
bromoethyl-2-benzyl ether

: 1427184-26-6
5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0 °C

1.2: Reflux

2.1: potassium hydrogencarbonate / acetonitrile / 25 °C

3.1: sodium tetrahydroborate / methanol / Reflux

4.1: acetone / 25 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 22 h / 25 °C

With 1H-imidazole; sodium tetrahydroborate; sodium hydride; potassium hydrogencarbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 172644-49-4
4-benzyloxy-2,2-dihydroxymethylbutanol

: 1427184-26-6
5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 25 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 22 h / 25 °C

With 1H-imidazole; In N,N-dimethyl-formamide; acetone;