5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane

Base Information

Chemical Name:5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane
CAS No.:1427184-27-7
Molecular Formula:C₂₅H₃₆O₄Si
Molecular Weight:428.644
Hs Code.:

Synonyms:5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane

Chemical Property:

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Technology Process of 5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane

There total 4 articles about 5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427184-26-6
5-benzyloxyethyl-2,2-dimethyl-5-(t-butyldiphenylsiloxymethyl)-1,3-dioxane

: 1427184-27-7
5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethyl acetate; at 25 ℃; for 22h; Inert atmosphere;

Reference yield:

: 172644-48-3
diethyl 2-(2-benzyloxyethyl)-2-hydroxymethylmalonate

: 1427184-27-7
5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol / Reflux

2: acetone / 25 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 22 h / 25 °C

4: palladium on activated charcoal; hydrogen / ethyl acetate / 22 h / 25 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; palladium on activated charcoal; hydrogen; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetone;

Reference yield:

: 172644-49-4
4-benzyloxy-2,2-dihydroxymethylbutanol

: 1427184-27-7
5-(t-butyldiphenylsiloxymethyl)-2,2-dimethyl-5-hydroxyethyl-1,3-dioxane

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 25 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 22 h / 25 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 22 h / 25 °C / Inert atmosphere

With 1H-imidazole; palladium on activated charcoal; hydrogen; In ethyl acetate; N,N-dimethyl-formamide; acetone;