di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

Base Information

Chemical Name:di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate
CAS No.:1446011-79-5
Molecular Formula:C₃₂H₅₂N₁₀O₆S
Molecular Weight:704.894
Hs Code.:

Synonyms:di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

Suppliers and Price of di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

There total 2 articles about di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1446011-78-4
4-(2-(di(prop-2-yn-1-yl)amino)ethyl)benzenesulfonamide

: 129392-85-4
N-t-butoxycarbonyl-4-azidobutylamine

: 1446011-79-5
di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

Guidance literature:: With copper; copper(II) sulfate; In tetrahydrofuran; water; at 20 ℃;

Reference yield:

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1446011-79-5
di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile; toluene / 20 °C

2: copper; copper(II) sulfate / tetrahydrofuran; water / 20 °C

With copper; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; toluene; acetonitrile;

Reference yield: 53.0%

: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]

: 1446011-79-5
di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate

: 1446011-61-5
C₂₅H₃₆N₁₀O₅ReS⁽¹⁺⁾

Guidance literature:: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]; di-tert-butyl ((4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))bis(butane-4,1-diyl))dicarbamate; In acetonitrile; at 90 ℃; for 4h; Inert atmosphere; Autoclave;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;