3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin

Base Information

Chemical Name:3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin
CAS No.:160641-61-2
Molecular Formula:C₁₅H₉BrCl₃N₃O₃
Molecular Weight:465.518
Hs Code.:

Synonyms:3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin

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Technology Process of 3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin

There total 6 articles about 3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 160647-14-3
8-(2,4,6-Trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridine

: 160641-61-2
3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin

Guidance literature:: With N-Bromosuccinimide; In ethanol;
DOI:10.1021/jm970591c

Reference yield:

: 50-43-1
2,4,6-trichlorobenzoic acid

: 160641-61-2
3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin

Guidance literature:: Multi-step reaction with 5 steps

1: 70percent aq. HNO₃, H₂SO₄ / 1.5 h / 10 °C

2: NaBH₄ / methanol / 1 h / 10 °C

3: Et₃N / CH₂Cl₂

4: K₂CO₃ / dimethylformamide / 2 h / Ambient temperature

5: N-bromosuccinimide / ethanol

With sodium tetrahydroborate; N-Bromosuccinimide; sulfuric acid; nitric acid; potassium carbonate; triethylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm970591c

Reference yield:

: 71372-03-7
2,4,6-trichloro-3-nitrobenzoic acid

: 160641-61-2
3-Bromo-8-(2,4,6-trichloro-3-nitrobenzyloxy)-2-methylimidazo[1,2-a]pyridin

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / methanol / 1 h / 10 °C

2: Et₃N / CH₂Cl₂

3: K₂CO₃ / dimethylformamide / 2 h / Ambient temperature

4: N-bromosuccinimide / ethanol

With sodium tetrahydroborate; N-Bromosuccinimide; potassium carbonate; triethylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm970591c