phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester

Base Information

Chemical Name:phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester
CAS No.:926919-36-0
Molecular Formula:C₂₆H₂₄F₃O₇P
Molecular Weight:536.441
Hs Code.:

Synonyms:phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester

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Chemical Property of phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester

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Technology Process of phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester

There total 3 articles about phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 926919-35-9
5-(bis-benzyloxy-phosphoryloxymethyl)-2-phenyl-[1,3]dioxolane-4-carboxylic acid methyl ester

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 926919-36-0
phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: 5-(bis-benzyloxy-phosphoryloxymethyl)-2-phenyl-[1,3]dioxolane-4-carboxylic acid methyl ester; (trifluoromethyl)trimethylsilane; With cesium fluoride;

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2006.11.091

Reference yield:

: 926919-34-8
5-hydroxymethyl-2-phenyl-[1,3]dioxolane-4-carboxylic acid methyl ester

: 926919-36-0
phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 81 percent / tetrazole; mCPBA / CH₂Cl₂

2.1: cesium fluoride

2.2: 70 percent / tetrabutylammonium fluoride / tetrahydrofuran

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; cesium fluoride; In dichloromethane;
DOI:10.1016/j.tetlet.2006.11.091

Reference yield:

: 38270-72-3
dimethyl 2,3-O-benzylidene-L-tartrate

: 926919-36-0
phosphoric acid dibenzyl ester 2-phenyl-5-trifluoroacetyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / NabH₄ / methanol

2.1: 81 percent / tetrazole; mCPBA / CH₂Cl₂

3.1: cesium fluoride

3.2: 70 percent / tetrabutylammonium fluoride / tetrahydrofuran

With 1H-tetrazole; sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; cesium fluoride; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2006.11.091