C₂₁H₂₂BrNO₃S

Base Information

Chemical Name:C₂₁H₂₂BrNO₃S
CAS No.:1437301-96-6
Molecular Formula:C₂₁H₂₂BrNO₃S
Molecular Weight:448.381
Hs Code.:

C<sub>21</sub>H<sub>22</sub>BrNO<sub>3</sub>S

Synonyms:C₂₁H₂₂BrNO₃S

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Chemical Property of C₂₁H₂₂BrNO₃S

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Technology Process of C₂₁H₂₂BrNO₃S

There total 4 articles about C₂₁H₂₂BrNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₆BrNO₄S

: 1437301-96-6
C₂₁H₂₂BrNO₃S

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 0.5h;
DOI:10.1021/ol4007713

Reference yield:

: 1437301-95-5
C₂₂H₂₄BrNO₂S

: 1437301-96-6
C₂₁H₂₂BrNO₃S

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methylmorpholine 4-oxide monohydrate / acetone; water / 0.17 h / 20 °C

1.2: 20 °C

2.1: sodium periodate / tetrahydrofuran; water / 0.5 h / 20 °C

With sodium periodate; 4-methylmorpholine 4-oxide monohydrate; In tetrahydrofuran; water; acetone;
DOI:10.1021/ol4007713

Reference yield:

: 1024-38-0
N-(2-bromophenyl)-4-methylbenzenesulfonamide

: 1437301-96-6
C₂₁H₂₂BrNO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

2.1: 4-methylmorpholine 4-oxide monohydrate / acetone; water / 0.17 h / 20 °C

2.2: 20 °C

3.1: sodium periodate / tetrahydrofuran; water / 0.5 h / 20 °C

With sodium periodate; di-isopropyl azodicarboxylate; 4-methylmorpholine 4-oxide monohydrate; triphenylphosphine; In tetrahydrofuran; water; acetone; 1.1: |Mitsunobu Displacement;
DOI:10.1021/ol4007713