C₂₇H₂₆F₃NO₃

Base Information

Chemical Name:C₂₇H₂₆F₃NO₃
CAS No.:226914-91-6
Molecular Formula:C₂₇H₂₆F₃NO₃
Molecular Weight:469.504
Hs Code.:

C<sub>27</sub>H<sub>26</sub>F<sub>3</sub>NO<sub>3</sub>

Synonyms:C₂₇H₂₆F₃NO₃

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Chemical Property of C₂₇H₂₆F₃NO₃

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Technology Process of C₂₇H₂₆F₃NO₃

There total 18 articles about C₂₇H₂₆F₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₂₈F₃NO₃*ClH

: 226914-91-6
C₂₇H₂₆F₃NO₃

Guidance literature:: With Jones reagent; In acetone; at 20 ℃;

Reference yield:

: C₂₉H₃₀NO₄F₃

: 226914-91-6
C₂₇H₂₆F₃NO₃

Guidance literature:: With hydrogenchloride; In acetone; at 50 ℃;
DOI:10.1021/jm061043e

Reference yield:

: 226915-53-3
(2R)-4-hydroxypentyl-2-ynoic acid benzyl ester

: 226914-91-6
C₂₇H₂₆F₃NO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: H₂ / Lindlar's catalyst / tetrahydrofuran / 2.5 h / 760.05 Torr

2.1: 1,3-dicyclohexylcarbodiimide; 4-pyrrolidinopyridine / CH₂Cl₂ / 0 °C

2.2: CH₂Cl₂ / 0 - 20 °C

3.1: xylene / 215 °C

4.1: DBU / tetrahydrofuran

5.1: H₂ / Pd/C / ethyl acetate / 760.05 Torr

6.1: thionyl chloride / toluene / 80 °C

7.1: tributyltin hydride / Pd(Ph₃P)4 / toluene / 0 °C

8.1: n-BuLi / tetrahydrofuran; hexane / 0 °C

8.2: tetrahydrofuran; hexane / 0 °C

9.1: aq. HCl / acetone / 50 °C

With hydrogenchloride; n-butyllithium; thionyl chloride; hydrogen; tri-n-butyl-tin hydride; 4-pyrrolidin-1-ylpyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; palladium on activated charcoal; Lindlar's catalyst; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; acetone; toluene; xylene; 3.1: Diels-Alder reaction / 8.2: Horner-Emmons reaction;
DOI:10.1021/jm061043e