hydridochlorocarbonyltris(triphenylarsine)osmium(II)

Base Information

Chemical Name:hydridochlorocarbonyltris(triphenylarsine)osmium(II)
CAS No.:55802-01-2
Molecular Formula:C₅₅H₄₆As₃ClOOs
Molecular Weight:1173.39
Hs Code.:

Synonyms:hydridochlorocarbonyltris(triphenylarsine)osmium(II)

Suppliers and Price of hydridochlorocarbonyltris(triphenylarsine)osmium(II)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of hydridochlorocarbonyltris(triphenylarsine)osmium(II)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of hydridochlorocarbonyltris(triphenylarsine)osmium(II)

There total 1 articles about hydridochlorocarbonyltris(triphenylarsine)osmium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: sodium hexachloroosmate hexahydrate

: 603-32-7
triphenyl-arsane

: 55802-01-2
carbonylchlorohydridotris(triphenylarsine)osmium(II)

Guidance literature:: With formaldehyd; triethylamine; In 2-methoxy-ethanol; water; addn. of soln. of Os-complex in methoxyethanol, aq. CH2O (40 %) and Et3N to boiled and stirred soln. of Ph3As in methoxyethanol, refluxing (1 h; pptn.); cooling to room temp., collection, washing (MeOH, H2O,MeOH, hexane), drying (vac.); elem. anal.;
DOI:10.1016/S0020-1693(00)88880-5

Reference yield: 91.0%

: 55802-01-2
carbonylchlorohydridotris(triphenylarsine)osmium(II)

: 75455-87-7
chlorohydridodicarbonylbis(triphenylarsine)osmium(II)

Guidance literature:: With carbon monoxide; In benzene; refluxing with bubbling CO (1 h); solvent removal, dissolving (CH2Cl2), pptn. on MeOH addn., collecting, washing (MeOH, hexane); elem. anal.;
DOI:10.1016/S0020-1693(00)88880-5