N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate

Base Information

Chemical Name:N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate
CAS No.:851539-75-8
Molecular Formula:C₃₃H₃₇N₂OPd*F₆Sb
Molecular Weight:819.83
Hs Code.:

Synonyms:N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate

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Chemical Property of N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate

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Technology Process of N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate

There total 1 articles about N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 26042-64-8
silver hexafluoroantimonate

: 851539-74-7
N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II) methyl iodide

: 851539-75-8
N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate

Guidance literature:: In diethyl ether; dichloromethane; byproducts: AgI; (Ar), Pd complex and AgSbF6 cooled to -78°C, slowly treated with CH2Cl2 and ether; filtered at -78°C, treated with ether, evapd.(vac.) at -10°C, ether added, filtered, concd.(vac.), solid dried (vac.) at -40°C for 2 h;
DOI:10.1021/ja045969s

Reference yield:

: 433-28-3,25748-85-0
trifluoro-acetic acid vinyl ester

: 851539-75-8
N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(diethyl ether) hexafluoroantimonate

: N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(η2-vinyl trifluoroacetate) hexafluoroantimonate

Guidance literature:: In dichloromethane-d2; (Ar), in NMR tube, Pd complex and AgSbF6 cooled to -78°C, slowly treated with CD2Cl2 and vinyl acetate, vivorously shaked; not isolated, detected by NMR; Kinetics;
DOI:10.1021/ja045969s