Z-Asnα-(Ac3GlcNAc)βLeuThrNH2

Base Information

Chemical Name:Z-Asnα-(Ac3GlcNAc)βLeuThrNH2
CAS No.:129835-79-6
Molecular Formula:C₃₆H₅₂N₆O₁₅
Molecular Weight:808.84
Hs Code.:

Synonyms:Z-Asnα-(Ac3GlcNAc)βLeuThrNH2

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Chemical Property of Z-Asnα-(Ac3GlcNAc)βLeuThrNH2

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Technology Process of Z-Asnα-(Ac3GlcNAc)βLeuThrNH2

There total 4 articles about Z-Asnα-(Ac3GlcNAc)βLeuThrNH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 75671-57-7
H-Leu-Thr-NH₂*TFA

: 38877-35-9
Z-Asnα-(Ac3GlcNAc)β-OH

: 129835-79-6
Z-Asnα-(Ac3GlcNAc)βLeuThrNH2

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1) - 10 deg C, 30 min, 2) r.t., 15 h;
DOI:10.1021/jo00313a013

Reference yield:

: 4515-24-6
2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine

: 129835-79-6
Z-Asnα-(Ac3GlcNAc)βLeuThrNH2

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / tetrahydrofuran / 1) - 10 deg C, 30 min, 2) r.t., 15 h

2: 78 percent / TFA / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 75 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / tetrahydrofuran / 1) - 10 deg C, 30 min, 2) r.t., 15 h

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00313a013

Reference yield:

: 129835-78-5
Z-Asnα-(Ac3GlcNAc)β-OBu^t

: 129835-79-6
Z-Asnα-(Ac3GlcNAc)βLeuThrNH2

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / TFA / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 75 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / tetrahydrofuran / 1) - 10 deg C, 30 min, 2) r.t., 15 h

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00313a013