Technology Process of C42H51N5O6Si
There total 26 articles about C42H51N5O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; water;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 14h;
DOI:10.1002/anie.201008079
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C
2: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere
3: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C
4: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C
With
pyridine; hydrogenchloride; dmap; trifluoromethylsulfonic anhydride; water; triethylamine; ytterbium(III) triflate;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/anie.201008079
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: zinc trifluoromethanesulfonate; acetic acid / 48 h / 80 °C
1.2: 1 h / 0 - 20 °C
2.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C
3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere
4.1: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C
5.1: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C
With
pyridine; hydrogenchloride; dmap; trifluoromethylsulfonic anhydride; water; zinc trifluoromethanesulfonate; acetic acid; triethylamine; ytterbium(III) triflate;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/anie.201008079