2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester

Base Information

• Chemical Name: 2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester
• CAS No.: 78647-36-6
• Molecular Formula: C₂₄H₃₀O₆S
• Molecular Weight: 446.565

Synonyms:2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester

Chemical Property of 2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester

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Technology Process of 2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester

There total 2 articles about 2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

carbon monoxide (201230-82-2) + 2-(4-hydroxypentyl)-1,3-dioxolane (78647-35-5) + 1-iodo-2-phenylthiomethyl-4,6-dimethoxy-benzene (74726-78-6) → 2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester (78647-36-6)

Guidance literature:

With triethylamine; palladium dichloride; In benzene; at 100 ℃; for 13h;

DOI:10.1016/S0040-4039(01)90320-X

Reference yield:

hex-5-en-1-al (764-59-0) → 2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester (78647-36-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 70 percent / Et₃N / PdCl₂ / benzene / 13 h / 100 °C

With triethylamine; palladium dichloride; In benzene;

DOI:10.1016/S0040-4039(01)90320-X

Reference yield: 90.0%

tetramethylene iodohydrin EE ether (78647-37-7) + 2,4-Dimethoxy-6-phenylsulfanylmethyl-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester (78647-36-6) → 2-[5-(1-Ethoxy-ethoxy)-1-phenylsulfanyl-pentyl]-4,6-dimethoxy-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester (78647-38-8)

Guidance literature:

With potassium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃;

DOI:10.1016/S0040-4039(01)90320-X

upstream raw materials:

carbon monoxide

2-(4-hydroxypentyl)-1,3-dioxolane

1-iodo-2-phenylthiomethyl-4,6-dimethoxy-benzene

hex-5-en-1-al

Downstream raw materials:

2-[5-(1-Ethoxy-ethoxy)-1-phenylsulfanyl-pentyl]-4,6-dimethoxy-benzoic acid 4-[1,3]dioxolan-2-yl-1-methyl-butyl ester

Zearalenone Dimethyl Ether

2-((E)-5-Hydroxy-pent-1-enyl)-4,6-dimethoxy-benzoic acid 1-methyl-5-oxo-pentyl ester

2,4-Dimethoxy-6-[(E)-5-(toluene-4-sulfonyloxy)-pent-1-enyl]-benzoic acid 1-methyl-5-oxo-pentyl ester

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