(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

Base Information

Chemical Name:(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine
CAS No.:129611-57-0
Molecular Formula:C₃₅H₃₅NO₆
Molecular Weight:565.666
Hs Code.:

Synonyms:(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

Suppliers and Price of (2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

There total 3 articles about (2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120810-76-6
(2S,4S,5R)-4-Methyl-2-((E)-3-oxo-propenyl)-5-phenyl-oxazolidine-3-carboxylic acid benzyl ester

: 129611-57-0
(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 78.5 percent / NaClO₂, NaH₂PO₄ / H₂O; 2-methyl-propan-2-ol; various solvent(s) / Ambient temperature

2: 1. KOH, 2. Bu₄NHSO₄ / 1. methanol, RT, 5min; 2. CH₃CN, RT, overnight

3: 1. KH / 2. THF, RT, 18h; or with NaH

With potassium hydroxide; sodium chlorite; sodium dihydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate; potassium hydride; In water; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)89766-0

Reference yield:

: 129611-51-4
(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(E)-2-carboxy>ethyloxazolidine

: 129611-57-0
(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1. KOH, 2. Bu₄NHSO₄ / 1. methanol, RT, 5min; 2. CH₃CN, RT, overnight

2: 1. KH / 2. THF, RT, 18h; or with NaH

With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium hydride;
DOI:10.1016/S0040-4020(01)89766-0

Reference yield:

: 129611-52-5
(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(E)-2-carbobenzyloxy>ethyloxazolidine

: 100-51-6,185532-71-2
benzyl alcohol

: 129611-57-0
(2S,4S,5R)-4-Methyl-5-phenyl-3-carbobenzyloxy-2-<(1S)-1-benzyloxy-2-carbobenzyloxy>ethyloxazolidine

Guidance literature:: With potassium hydride; Yield given. Multistep reaction; 2. THF, RT, 18h; or with NaH;
DOI:10.1016/S0040-4020(01)89766-0