4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol

Base Information

• Chemical Name: 4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol
• CAS No.: 152980-18-2
• Molecular Formula: C₃₁H₃₅NO₂Si
• Molecular Weight: 481.71
• Mol file: 152980-18-2.mol

Synonyms:4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol

Chemical Property of 4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol

There total 1 articles about 4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1H-imidazole (288-32-4) + 2,3,5-trimethyl-6-(3-pyridylmethyl)-1,4-benzoquinone (117574-40-0) + tert-butylchlorodiphenylsilane (58479-61-1) → 4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol (152980-18-2)

Guidance literature:

With sodium dithionite; In dichloromethane; water;

Reference yield:

4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol (152980-18-2) + acetyl chloride (75-36-5) → 1-acetoxy-4-hydroxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylbenzene

Guidance literature:

With pyridine; tetra-n-butylammoniumfluoride trihydrate; In tetrahydrofuran; dichloromethane;

Reference yield:

boron trifluoride diethyl ether + 4-tert-butyldiphenylsilyloxy-6-(pyridin-3-ylmethyl)-2,3,5-trimethylphenol (152980-18-2) + methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate (92420-89-8) → Sodium 1-O-[4-hydroxy-6-(3-pyridylmethyl)-2,3,5-trimethylphenyl]-β-D-glucopyranosiduronate (152980-19-3)

Guidance literature:

With sodium hydroxide; sodium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; water;

upstream raw materials:

1H-imidazole

2,3,5-trimethyl-6-(3-pyridylmethyl)-1,4-benzoquinone

tert-butylchlorodiphenylsilane

Downstream raw materials:

Sodium 1-O-[4-hydroxy-6-(3-pyridylmethyl)-2,3,5-trimethylphenyl]-β-D-glucopyranosiduronate

Refernces