Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}

Base Information

Chemical Name:Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}
CAS No.:121064-38-8
Molecular Formula:C₃₀H₄₆N₄O₆
Molecular Weight:558.718
Hs Code.:

Synonyms:Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}

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Chemical Property of Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}

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Technology Process of Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}

There total 5 articles about Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 106163-12-6,106163-27-3
Hexanedioic acid bis-({4-[3-(benzyl-isopropyl-amino)-2-hydroxy-propoxy]-phenyl}-amide)

: 121064-38-8
Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}

Guidance literature:: With acetic acid; palladium on activated charcoal; In methanol; Ambient temperature;
DOI:10.1021/jm00387a025

Reference yield:

: 6597-75-7
1-(4-acetamidophenoxy)-2,3-epoxypropane

: 121064-38-8
Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / methanol / 5 h / Heating

2: 82.5 percent / HCl / ethanol / 5 h / Heating

3: 77 percent / triethylamine / diethyl ether / 3 h / Ambient temperature

4: 30 percent / 10percent HOAc / 5percent Pd/C / methanol / Ambient temperature

With hydrogenchloride; acetic acid; triethylamine; palladium on activated charcoal; In methanol; diethyl ether; ethanol;
DOI:10.1021/jm00387a025

Reference yield:

: 103-90-2,8055-08-1
4-acetaminophenol

: 121064-38-8
Hexanedioic acid bis-{[4-(2-hydroxy-3-isopropylamino-propoxy)-phenyl]-amide}

Guidance literature:: Multi-step reaction with 5 steps

1: 50 percent / NaOH / H₂O / 16 h / Ambient temperature

2: 89 percent / methanol / 5 h / Heating

3: 82.5 percent / HCl / ethanol / 5 h / Heating

4: 77 percent / triethylamine / diethyl ether / 3 h / Ambient temperature

5: 30 percent / 10percent HOAc / 5percent Pd/C / methanol / Ambient temperature

With hydrogenchloride; sodium hydroxide; acetic acid; triethylamine; palladium on activated charcoal; In methanol; diethyl ether; ethanol; water;
DOI:10.1021/jm00387a025