N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

Base Information

Chemical Name:N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine
CAS No.:940941-88-8
Molecular Formula:C₁₉H₂₄BrNSSi
Molecular Weight:406.462
Hs Code.:

Synonyms:N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

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Technology Process of N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

There total 1 articles about N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 867218-80-2
chloro(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilane

: 41825-73-4
2-bromo-4,6-dimethylaniline

: 940941-88-8
N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

Guidance literature:: 2-bromo-4,6-dimethylaniline; With n-butyllithium; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 1h;

chloro(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilane; In tetrahydrofuran; hexane; at 20 ℃;

Reference yield: 20.0%

: 940941-88-8
N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

: 7550-45-0
titanium tetrachloride

: dimethylsilanediyl(η5-4,5-dimethylcyclopenta[b]thien-6-yl)(N-(2,4-dimethyl-6-bromophenylamido))titanium dichloride

Guidance literature:: N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine; With methyllithium; In diethyl ether; at 20 ℃;

titanium tetrachloride; In diethyl ether; pentane; at 0 - 20 ℃; for 24.5h;

Reference yield: 10.0%

: ZrCl₄(THF)2

: 940941-88-8
N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

: dimethylsilanediyl(η5-4,5-dimethylcyclopenta[b]thien-6-yl)(N-(2,4-dimethyl-6-bromophenylamido))zirconium dichloride

Guidance literature:: N-(2-bromo-4,6-dimethylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine; With methyllithium; In diethyl ether; at -50 ℃; for 12.1667h;

ZrCl₄(THF)2; In diethyl ether; at -80 ℃; for 24h;