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7550-45-0 Usage

Check Digit Verification of cas no

The CAS Registry Mumber 7550-45-0 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 7,5,5 and 0 respectively; the second part has 2 digits, 4 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 7550-45:
(6*7)+(5*5)+(4*5)+(3*0)+(2*4)+(1*5)=100
100 % 10 = 0
So 7550-45-0 is a valid CAS Registry Number.
InChI:InChI=1/4ClH.Ti/h4*1H;/q;;;;+4/p-4

7550-45-0 Well-known Company Product Price

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  • TCI America

  • (T2052)  Titanium(IV) Chloride (14% in Dichloromethane, ca. 1.0mol/L)  

  • 7550-45-0

  • 100mL

  • 375.00CNY

  • Detail
  • TCI America

  • (T2052)  Titanium(IV) Chloride (14% in Dichloromethane, ca. 1.0mol/L)  

  • 7550-45-0

  • 500mL

  • 1,290.00CNY

  • Detail
  • Alfa Aesar

  • (H31830)  Titanium(IV) chloride, 1M soln. in dichloromethane   

  • 7550-45-0

  • 100ml

  • 690.0CNY

  • Detail
  • Alfa Aesar

  • (H31830)  Titanium(IV) chloride, 1M soln. in dichloromethane   

  • 7550-45-0

  • 500ml

  • 1080.0CNY

  • Detail
  • Alfa Aesar

  • (H31808)  Titanium(IV) chloride, 1M soln. in toluene   

  • 7550-45-0

  • 100ml

  • 591.0CNY

  • Detail
  • Alfa Aesar

  • (H31808)  Titanium(IV) chloride, 1M soln. in toluene   

  • 7550-45-0

  • 500ml

  • 1979.0CNY

  • Detail
  • Alfa Aesar

  • (14713)  Titanium(IV) chloride, 99.0% min, typically 99.6%   

  • 7550-45-0

  • 100ml

  • 233.0CNY

  • Detail
  • Alfa Aesar

  • (14713)  Titanium(IV) chloride, 99.0% min, typically 99.6%   

  • 7550-45-0

  • 1L

  • 685.0CNY

  • Detail
  • Alfa Aesar

  • (14713)  Titanium(IV) chloride, 99.0% min, typically 99.6%   

  • 7550-45-0

  • *3x1L

  • 1857.0CNY

  • Detail
  • Alfa Aesar

  • (14713)  Titanium(IV) chloride, 99.0% min, typically 99.6%   

  • 7550-45-0

  • *3x1L

  • 2145.0CNY

  • Detail
  • Alfa Aesar

  • (22979)  Titanium(IV) chloride, 99.99% (metals basis)   

  • 7550-45-0

  • 2.5g

  • 81.0CNY

  • Detail
  • Alfa Aesar

  • (22979)  Titanium(IV) chloride, 99.99% (metals basis)   

  • 7550-45-0

  • 25g

  • 450.0CNY

  • Detail

7550-45-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Titanium(IV) chloride

1.2 Other means of identification

Product number -
Other names Titanium tetrachloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:7550-45-0 SDS

7550-45-0Synthetic route

titanium(IV) oxide

titanium(IV) oxide

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
TiO2 contained with 2%MnO2; chlorination at 600°C;96.08%
TiO2 contained with 2%MnO2; chlorination at 700°C;96.68%
TiO2 contained with 2%MnO2; chlorination at 600°C;96.08%
titanomagnetite FeTiO3#Fe3O4

titanomagnetite FeTiO3#Fe3O4

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
chlorination at 740°C;95.58%
chlorination at 640°C;79.52%
chlorination at 520°C;68.51%
titanite

titanite

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
chlorination at 850°C;28%
chlorination at 740°C;25.1%
chlorination at 640°C;13.1%
chloroform
67-66-3

chloroform

titanium oxide

titanium oxide

A

hydrogenchloride
7647-01-0

hydrogenchloride

B

hexachlorobenzene
118-74-1

hexachlorobenzene

C

titanium tetrachloride
7550-45-0

titanium tetrachloride

D

CO

CO

iron(III) oxide

iron(III) oxide

chlorine
7782-50-5

chlorine

pyrographite
7440-44-0

pyrographite

titanium(IV) oxide

titanium(IV) oxide

A

Fe2Cl6

Fe2Cl6

B

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: CO; TiO2/C mixt. (various ratio) heating in thermogravimetric analyzer at 2.7 K/min in Ar flow, Cl2 (p(Cl2)=33 kPa) introducing at 598 K, further heating up to 1000 K; TG;
disulfur dichloride
10025-67-9

disulfur dichloride

titanium(IV) oxide

titanium(IV) oxide

chlorine
7782-50-5

chlorine

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) chlorination (molar ratio SCl4:TiO2 = 2:1);
titanium carbide

titanium carbide

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
chlorination; distilling, shaking with Na-amalgame for 48h in dry H2;
chlorination; distilling, shaking with Na-amalgame for 48h in dry H2;
titanium carbide

titanium carbide

chlorine
7782-50-5

chlorine

A

titanium tetrachloride
7550-45-0

titanium tetrachloride

B

pyrographite
7440-44-0

pyrographite

Conditions
ConditionsYield
In neat (no solvent) chlorination (fused silica reactor, 773, 973, 1173, and 1373 K, Cl2 velocity 1 cm/s); removal of Cl2 and TiCl4 on heat treatment (synthesis temp., vac., 1 h);A n/a
B >99
hydrogenchloride
7647-01-0

hydrogenchloride

titanium nitride

titanium nitride

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: H2, N2, TiCl3; transport reaction; small reaction rate at 1000°C, high reaction rate at 1500°C;;
byproducts: NH3; dry HCl is used;;
byproducts: NH3; dry HCl is used;;
In neat (no solvent) byproducts: H2, N2, TiCl3; transport reaction; small reaction rate at 1000°C, high reaction rate at 1500°C;;
phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

ilmenite

ilmenite

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: POCl3, FeCl2; passing vapor of PCl5 over hot ilmenite;;
titanium
7440-32-6

titanium

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
With chlorine glowing;
With chlorine 325 ° C;
With chlorine finely dispersed Ti at 30 °C with clean, dry Cl2 gas or Cl2 gas contg. less than 0.005% water;
hydrogenchloride
7647-01-0

hydrogenchloride

titanium
7440-32-6

titanium

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) a stream of water-free HCl is used;;
titanium(IV) oxide

titanium(IV) oxide

calcium chloride

calcium chloride

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In melt berillium oxide crucible with TiO2 and CaCl2 heated at 840°C for 2.5 h; TiCl4 vapor condencat not observed;0%
phosgene
75-44-5

phosgene

titanium(IV) oxide

titanium(IV) oxide

A

titanium oxychloride

titanium oxychloride

B

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) passing stream of COCl2 over TiO2 at 450 °C;;
boron trichloride
10294-34-5

boron trichloride

titanium(IV) oxide

titanium(IV) oxide

A

boron trioxide

boron trioxide

B

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
higher temp. in Pt pot;
higher temp. in Pt pot;
chloroform
67-66-3

chloroform

titanium(IV) oxide

titanium(IV) oxide

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
byproducts: CO, HCl;
byproducts: CO, HCl;
titanium(IV) iodide
7720-83-4

titanium(IV) iodide

phosphorus trichloride
7719-12-2, 52843-90-0

phosphorus trichloride

A

phosphorous triiodide
13455-01-1

phosphorous triiodide

B

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
In not given react. with TiI4;;
In not given react. with TiI4;;
rutile

rutile

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
byproducts: FeCl3; red heat, chlorination;
With tetrachloromethane red heat, in tube;
With COCl2 600 °C;
2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol
757244-92-1

2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol

titanium tetrachloride
7550-45-0

titanium tetrachloride

dichloro{1-monothiaethanediyl-2,2'-bis(6-tert-butyl-4-methylphenolate)}titanium

dichloro{1-monothiaethanediyl-2,2'-bis(6-tert-butyl-4-methylphenolate)}titanium

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 0.5h;100%
water
7732-18-5

water

titanium tetrachloride
7550-45-0

titanium tetrachloride

titanium(IV) oxide

titanium(IV) oxide

Conditions
ConditionsYield
TiCl4 was added to deionized H2O, mixt. was stirred for 16 h at room temp., mixt was dialyzed in deionized H2O to pH 2.0;100%
In hydrogenchloride other Radiation; soln. of TiCl4 in cold 2 M HCl, hydrolysed, TiOCl2 formed, soln. transferred to Teflon container, treated in microwave oven (2.45 GHz) at temp. of 120°C for 120 min, or at 140°C for 60 or 120 min, or at160°C for 5 or 30 min; washed (deionized H2O, ethanol, repeatedly), dried in oven at 60°C for 16 h, detd. by XRD, mixt. of rutile and anatase obtained;99%
In hydrogenchloride other Radiation; soln. of TiCl4 in cold 2 M HCl, hydrolysed, TiOCl2 formed, soln. transferred to Teflon container, treated in microwave oven (2.45 GHz) at temp. of 160°C for 60 min; washed (deionized H2O, ethanol, repeatedly), dried in oven at 60°C for 16 h, detd. by XRD, mixt. of rutile and anatase obtained;98%
trans-cyclopentane-1,2-diol
5057-99-8

trans-cyclopentane-1,2-diol

titanium tetrachloride
7550-45-0

titanium tetrachloride

C5H8(OTiCl3)2

C5H8(OTiCl3)2

Conditions
ConditionsYield
In dichloromethane (Ar), at 0°C, dropwise addn. of TiCl4 with stirring, stirred for 15 min, brought to 25°C, stirred for 45 min; evapd. in vacuo, elem. anal.;100%
N,N,N,N,-tetramethylethylenediamine
110-18-9

N,N,N,N,-tetramethylethylenediamine

titanium tetrachloride
7550-45-0

titanium tetrachloride

tetrachloro(N,N,N',N'-tetramethylethane-1,2-diamine)titanium(IV)
19033-22-8

tetrachloro(N,N,N',N'-tetramethylethane-1,2-diamine)titanium(IV)

Conditions
ConditionsYield
In hexane at 0℃; for 1h; Inert atmosphere;100%
In benzene solns. mixed at 10-20°C; filtered, washed (benzene), dried (vac.); elem. anal.;>99
In pentane solns. mixed at 10-20°C; filtered, washed (pentane), dried (vac.); elem. anal.;>99
α-naphthol
90-15-3

α-naphthol

titanium tetrachloride
7550-45-0

titanium tetrachloride

[dichlorobis(1-naphtholate)titanium(IV)]
104043-19-8

[dichlorobis(1-naphtholate)titanium(IV)]

Conditions
ConditionsYield
In toluene byproducts: HCl; N2, vigorously refluxed for 12 h; cooled, filtered, solvent removed;100%
1,3,5,7-tetrathiocane
2373-00-4

1,3,5,7-tetrathiocane

titanium tetrachloride
7550-45-0

titanium tetrachloride

TiCl4*2(CH2S)4

TiCl4*2(CH2S)4

Conditions
ConditionsYield
In benzene under moisture-free conditions; freshly distd. TiCl4 added to a soln. of thioaldehyde; mixt. stirred (2 h, room temp.); filtered; washed (pentane); dried (high vac., room temp.); elem. anal.;100%
2-{[(1-methylethyl)imino]methyl}phenol
5961-35-3

2-{[(1-methylethyl)imino]methyl}phenol

titanium tetrachloride
7550-45-0

titanium tetrachloride

bis(κN,κO-N-isopropylsalicylaldiminato)TiCl2
69046-27-1, 86322-28-3

bis(κN,κO-N-isopropylsalicylaldiminato)TiCl2

Conditions
ConditionsYield
With 1,1,1,3,3,3-hexamethyldisilazane In dichloromethane; toluene (under Ar, Schlenk); hexamethyldisilazane added to soln. of ligand in CH2Cl2, stirred overnight, evapd. under vac. at 50°C, ligand in toluene added to toluene soln. of TiCl4 at -78°C, warmed to ambient temp., stirred overnight; heated at 50°C under vac.; elem. anal.;100%
1,3,5,7,9-pentathiacyclodecane
2372-99-8

1,3,5,7,9-pentathiacyclodecane

titanium tetrachloride
7550-45-0

titanium tetrachloride

TiCl4*(CH2S)5
103602-01-3

TiCl4*(CH2S)5

Conditions
ConditionsYield
In benzene under moisture-free conditions; equimolar quantity of freshly distd. TiCl4 added to a soln. of thioaldehyde; mixt. stirred (2 h, room temp.); filtered; washed (pentane); dried (high vac., room temp.); elem. anal.;100%
6,6'-((1E,1'E)-(cyclohexane-1,2-diylbis(azanylylidene))bis(methanylylidene))bis(2-(tert-butyl)-4-nitrophenol)

6,6'-((1E,1'E)-(cyclohexane-1,2-diylbis(azanylylidene))bis(methanylylidene))bis(2-(tert-butyl)-4-nitrophenol)

titanium tetrachloride
7550-45-0

titanium tetrachloride

Ti(C28H34N4O6)Cl2

Ti(C28H34N4O6)Cl2

Conditions
ConditionsYield
In dichloromethane Ar-atmosphere; stirring of equiv. amts. of ligand and TiCl4 for 2 h at room temp.; concn. (vac.), washing (ether, ether/petroleum ether=1/1), recrystn. (CHCl3); elem. anal.;100%
N-(1-adamantyl)-salicylaldamine
54547-03-4

N-(1-adamantyl)-salicylaldamine

titanium tetrachloride
7550-45-0

titanium tetrachloride

bis(κN,κO-N-adamantylsalicylaldiminato)TiCl2
945831-77-6

bis(κN,κO-N-adamantylsalicylaldiminato)TiCl2

Conditions
ConditionsYield
With 1,1,1,3,3,3-hexamethyldisilazane In dichloromethane; toluene (under Ar, Schlenk); hexamethyldisilazane added to soln. of ligand in CH2Cl2, stirred overnight, evapd. under vac. at 50°C, ligand in toluene added to toluene soln. of TiCl4 at -78°C, warmed to ambient temp., stirred overnight; heated at 50°C under vac.; elem. anal.;100%
adamantyl-N-(3-tert-butylsalicylaldimine)
945831-89-0

adamantyl-N-(3-tert-butylsalicylaldimine)

titanium tetrachloride
7550-45-0

titanium tetrachloride

bis(κN,κO-N-adamantyl-3-tert-butylsalicylaldiminato)TiCl2
945831-79-8

bis(κN,κO-N-adamantyl-3-tert-butylsalicylaldiminato)TiCl2

Conditions
ConditionsYield
In toluene (under Ar, Schlenk); ligand in toluene added to toluene soln. of TiCl4 at -78°C, warmed to ambient temp., stirred overnight; elem. anal.;100%
C6H10(NCHC6H2(C(CH3)3)(NO2)OH)2

C6H10(NCHC6H2(C(CH3)3)(NO2)OH)2

titanium tetrachloride
7550-45-0

titanium tetrachloride

(C6H10(NCHC6H2(NO2)(C(CH3)3)O)2)TiCl2

(C6H10(NCHC6H2(NO2)(C(CH3)3)O)2)TiCl2

Conditions
ConditionsYield
In dichloromethane ligand dissolved in CH2Cl2; soln. of TiCl4 in CH2Cl2 added; stirred for 1 h; solvent evapd. in vac.; taken up in Et2O; stirred for 5 min; ether layerdecanted; hexane-Et2O added to residue; stirred briefly; decanted; drie d in vac.;100%
HOC6H2Br2CH2N(CH3)C2H4NCHC6H2(OH)(C(CH3)3)2
1291070-42-2

HOC6H2Br2CH2N(CH3)C2H4NCHC6H2(OH)(C(CH3)3)2

titanium tetrachloride
7550-45-0

titanium tetrachloride

C25H32Br2Cl2N2O2Ti
1352912-54-9

C25H32Br2Cl2N2O2Ti

Conditions
ConditionsYield
In toluene for 0.25h;100%
C12H28N2O2
1403990-41-9

C12H28N2O2

titanium tetrachloride
7550-45-0

titanium tetrachloride

Conditions
ConditionsYield
With titanium(IV) isopropylate In toluene at -30℃;100%
C12H17NO2
1443157-01-4

C12H17NO2

titanium tetrachloride
7550-45-0

titanium tetrachloride

C24H34Cl4N2O4Ti
1443157-02-5

C24H34Cl4N2O4Ti

Conditions
ConditionsYield
In toluene Schlenk technique; Inert atmosphere; Glovebox;100%
tetrahydrofuran
109-99-9

tetrahydrofuran

C34H36N2O2

C34H36N2O2

titanium tetrachloride
7550-45-0

titanium tetrachloride

(x)C4H8O*C34H34N2O2(2-)*2Cl(1-)*Ti(4+)

(x)C4H8O*C34H34N2O2(2-)*2Cl(1-)*Ti(4+)

Conditions
ConditionsYield
Stage #1: tetrahydrofuran; C34H36N2O2 With n-butyllithium In hexane at -78 - 20℃; for 2.16667h;
Stage #2: titanium tetrachloride In hexane at -78 - 20℃; for 18.3333h;
100%
1-(2,6-diisopropylphenyl)-3-(2-hydroxyphenyl)-4,5-dihydro-imidazolyl chloride
724794-67-6

1-(2,6-diisopropylphenyl)-3-(2-hydroxyphenyl)-4,5-dihydro-imidazolyl chloride

titanium tetrachloride
7550-45-0

titanium tetrachloride

bis(1-(2,6-diisopropylphenyl)-3-(2-hydroxyphenyl)-4,5-dihydro-imidazolyl)titanium(IV) dichloride

bis(1-(2,6-diisopropylphenyl)-3-(2-hydroxyphenyl)-4,5-dihydro-imidazolyl)titanium(IV) dichloride

Conditions
ConditionsYield
Stage #1: 1-(2,6-diisopropylphenyl)-3-(2-hydroxyphenyl)-4,5-dihydroimidazolium chloride With potassium hexamethylsilazane In tetrahydrofuran at 20℃; for 0.166667h;
Stage #2: titanium tetrachloride In tetrahydrofuran; toluene at 20℃; for 2h;
100%
2,4,6-trimethyl-pyridine
108-75-8

2,4,6-trimethyl-pyridine

titanium tetrachloride
7550-45-0

titanium tetrachloride

TiCl4(2,4,6-collidine)

TiCl4(2,4,6-collidine)

Conditions
ConditionsYield
In hexane at 0℃; for 1h; Inert atmosphere;100%
C51H47NO2

C51H47NO2

titanium tetrachloride
7550-45-0

titanium tetrachloride

C51H45Cl2NO2Ti

C51H45Cl2NO2Ti

Conditions
ConditionsYield
In toluene at -78 - 20℃; for 21h; Schlenk technique; Inert atmosphere;100%
C59H73NO3

C59H73NO3

titanium tetrachloride
7550-45-0

titanium tetrachloride

C59H70ClNO3Ti

C59H70ClNO3Ti

Conditions
ConditionsYield
In toluene at -78 - 100℃; for 13h;99.4%
Butane-1,4-diol
110-63-4

Butane-1,4-diol

titanium tetrachloride
7550-45-0

titanium tetrachloride

C8H16O4Ti

C8H16O4Ti

Conditions
ConditionsYield
With calcium hydroxide for 2h; Autoclave; Cooling with ice; Inert atmosphere; Green chemistry;99.3%

7550-45-0Relevant articles and documents

Wardlaw, W.,Clews, F. H.

, p. 1093 - 1103 (1920)

Jakubec, I.,Vondrak, J.,Bludska, J.

, p. 447 - 452 (1989)

Jakubec, I.,Vondrak, J.,Bludska, J.

, p. 505 - 510 (1989)

Rhead, E. L.

, p. 1491 - 1495 (1906)

Heterogeneous Catalysis in Solution. Part 27. - Reaction between Titanium(III) and Triiodide Ions Catalysed by Platinum

Xiao, Shaorong,Spiro, Michael

, p. 1983 - 1986 (1994)

The rate of the reaction between titanium(III) chloride and triiodide ions in an acid chloride medium has been studied in the absence and presence of a rotating platinum disk.At low concentrations of triiodide the catalytic rate at platinum was found to be first order in I3(-), zero order with respect to Ti(III) and H(+), and proportional to the square root of the rotation speed of the disk.These results pointed to diffusion-controlled catalysis, as did the low activation energy of 19 kJ mol-1 as compared with 40 kJ mol-1 for the uncatalysed reaction.All these findings are consistent with an electrochemical interpretation of the catalytic mechanism, as was shown by the current-potential curves determined for the two reactants at the same reduced platinum surface.Provided that the voltammograms for Ti(III) had been carried out in the presence of the same concentration of KI as in the reaction mixtures, the rates and mixture potentials determined electrochemically agreed well with the catalytic rates and potentials measured experimentally.The fact that quite different results were obtained when no KI was present in the TiCl3 solution provides further confirmation for the modified form of the additivity principle.

The low temperature synthesis of metal oxides by novel hydrazine method

Rane,Uskaikar,Pednekar,Mhalsikar

, p. 627 - 638 (2008/10/09)

The hydroxide, oxalate and citrate precursors of the metal oxides such as γ-Fe2O3, (MnZn)Fe2O4, Cu(K)Fe2O4, BaTiO3, La(Sr)MnO3, La(Sr)AlO3, La/Gd(Ca/Ba/Sr)C

Electron deficient carbon-titanium triple bonds: Formation of triplet XC÷TiX3 methylidyne complexes

Lyon, Jonathan T.,Andrews, Lester

, p. 9858 - 9863 (2008/10/09)

Laser-ablated titanium atoms react with CX4 (X = F and Cl) to produce triplet state XC÷TiX3 complexes trapped in an argon matrix. Products are identified by their infrared spectra and comparison to theoretically predicted vibrations.

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