methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate

Base Information

Chemical Name:methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate
CAS No.:936111-62-5
Molecular Formula:C₃₀H₃₂F₂O₇
Molecular Weight:542.577
Hs Code.:

Synonyms:methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate

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Technology Process of methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate

There total 4 articles about methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 936111-61-4
C₃₀H₃₂F₂O₇

: 18107-18-1
diazomethyl-trimethyl-silane

: 936111-62-5
methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate

Guidance literature:: C₃₀H₃₂F₂O₇; With sodium methylate; In methanol; at 20 ℃; for 23h;

diazomethyl-trimethyl-silane; With methanol; In toluene; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1021/ol070169i

Reference yield: 52.0%

: 936111-61-4
C₃₀H₃₂F₂O₇

: 936111-62-5
methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate

: C₃₀H₃₂F₂O₇

Guidance literature:: C₃₀H₃₂F₂O₇; With sodium methylate; In methanol; at 20 ℃; for 23h;

With diazomethyl-trimethyl-silane; In methanol; diethyl ether; toluene; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.carres.2007.06.012

Reference yield:

: 936111-60-3
methyl (3S,4R,5S,6R)-4,5,6-tris(benzyloxy)-2,2-difluoro-3-hydroxyoct-7-enoate

: 936111-62-5
methyl 3,7-anhydro-4,5,6-tri-O-benzyl-2,2-difluoro-glycero-D-talo-octosonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 74 percent Turnov_. / m-CPBA; NaH₂PO₄ / CH₂Cl₂; H₂O / 26 h / 20 °C

2.1: sodium methylate / methanol / 23 h / 20 °C

2.2: 52 percent / methanol / toluene / 0.5 h / 0 °C

With sodium dihydrogenphosphate; sodium methylate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; water;
DOI:10.1021/ol070169i