5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one

Base Information

• Chemical Name: 5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one
• CAS No.: 87922-30-3
• Molecular Formula: C₂₀H₁₇NO₆
• Molecular Weight: 367.358

Synonyms:5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one

Chemical Property of 5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one

Chemical Property:

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Technology Process of 5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one

There total 3 articles about 5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

3t-benzo[1,3]dioxol-5-yl-6,7-dimethoxy-2-methyl-1-oxo-1,2,3,4-tetrahydro-isoquinoline-4r-carboxylic acid (64036-06-2) → N-methyl-3-<3,4-(methylenedioxy)phenyl>-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinoline (87922-31-4) + 5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one (87922-30-3)

Guidance literature:

at 220 ℃; for 4h;

DOI:10.1021/jm00370a021

Reference yield:

3,4-dimethoxyhomophthalic anhydride (5653-42-9) → 5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one (87922-30-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 25 percent / CHCl₃ / 0.5 h / Ambient temperature

2: 10 percent / 4 h / 220 °C

In chloroform;

DOI:10.1021/jm00370a021

Reference yield:

N-[(1E)-1,3-benzodioxol-5-ylmethylene]methanamine (113975-93-2) → 5,6-(methylenedioxy)-2-<2-(methylcarbamoyl)-4,5-dimethoxyphenyl>-1H-inden-1-one (87922-30-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 25 percent / CHCl₃ / 0.5 h / Ambient temperature

2: 10 percent / 4 h / 220 °C

In chloroform;

DOI:10.1021/jm00370a021

upstream raw materials:

3t-benzo[1,3]dioxol-5-yl-6,7-dimethoxy-2-methyl-1-oxo-1,2,3,4-tetrahydro-isoquinoline-4r-carboxylic acid

3,4-dimethoxyhomophthalic anhydride

N-[(1E)-1,3-benzodioxol-5-ylmethylene]methanamine

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