1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol

Base Information

• Chemical Name: 1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol
• CAS No.: 326093-86-1
• Molecular Formula: C₁₆H₁₅BrN₂O₂S
• Molecular Weight: 379.277

Synonyms:1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol

Chemical Property of 1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol

Chemical Property:

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Technology Process of 1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol

There total 4 articles about 1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanone (37052-85-0) → 1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol (326093-86-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; chloroform; at 20 ℃;

DOI:10.1016/S0223-5234(03)00144-2

Reference yield:

1-(4-bromophenyl)-2-chloroethan-1-one (4209-02-3) → 1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol (326093-86-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone

2: NaBH₄ / CHCl₃; methanol / 20 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; chloroform; acetone;

DOI:10.1016/S0223-5234(03)00144-2

Reference yield:

2-Mercapto-5-methoxybenzimidazole (37052-78-1) → 1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanol (326093-86-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone

2: NaBH₄ / CHCl₃; methanol / 20 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; chloroform; acetone;

DOI:10.1016/S0223-5234(03)00144-2

upstream raw materials:

1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazol-2-ylsulfanyl)-ethanone

1-(4-bromophenyl)-2-chloroethan-1-one

2-Mercapto-5-methoxybenzimidazole

4-methoxy-1,2-phenylenediamine

Downstream raw materials:

1-(4-bromo-phenyl)-2-(5-methoxy-1H-benzoimidazole-2-sulfonyl)-ethanol

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