6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

Base Information

Chemical Name:6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester
CAS No.:77628-08-1
Molecular Formula:C₂₉H₃₀N₂O₅S
Molecular Weight:518.634
Hs Code.:

Synonyms:6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

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Chemical Property of 6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

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Technology Process of 6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

There total 6 articles about 6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 21142-82-5
6L-carbobenzyloxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

: 908093-98-1
diazodiphenylmethane

: 77628-08-1
6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

Guidance literature:: In dichloromethane;
DOI:10.1139/v81-062

Reference yield:

: 21149-17-7
methyl 2-(benzyloxycarbonylamino)acrylate

: 77628-08-1
6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / triethylamine / methanol / 192 h / Ambient temperature

2: 79 percent / CH₂Cl₂

With triethylamine; In methanol; dichloromethane;
DOI:10.1139/v81-062

Reference yield:

: 3693-95-6
N,N'-bis[(phenylmethoxy)carbonyl]-L-cystine 1,1'-dimethyl ester

: 77628-08-1
6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / conc. hydrochloric acid, zinc / methanol / 0.25 h / 0 °C

2: 92 percent / Fetizon's reagent / methanol; H₂O / 8.5 h / Heating

3: 22 percent / triethylamine / methanol / 192 h / Ambient temperature

4: 79 percent / CH₂Cl₂

With hydrogenchloride; triethylamine; silver carbonate; zinc; In methanol; dichloromethane; water;
DOI:10.1139/v81-062