3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide

Base Information

Chemical Name:3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide
CAS No.:77628-12-7
Molecular Formula:C₂₉H₃₀N₂O₆S
Molecular Weight:534.633
Hs Code.:

Synonyms:3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide

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Chemical Property of 3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide

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Technology Process of 3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide

There total 7 articles about 3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 77628-08-1
6L-carbobenzoxyamino-3D-carboxy-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine benzhydryl ester

: 77628-12-7
3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 4 ℃; for 2.5h;
DOI:10.1139/v81-062

Reference yield:

: 21149-17-7
methyl 2-(benzyloxycarbonylamino)acrylate

: 77628-12-7
3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 22 percent / triethylamine / methanol / 192 h / Ambient temperature

2: 79 percent / CH₂Cl₂

3: 98 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 2.5 h / 4 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1139/v81-062

Reference yield:

: 3693-95-6
N,N'-bis[(phenylmethoxy)carbonyl]-L-cystine 1,1'-dimethyl ester

: 77628-12-7
3D-benzhydryloxycarbonyl-6L-carbobenzoxyamino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine-1-oxide

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / conc. hydrochloric acid, zinc / methanol / 0.25 h / 0 °C

2: 92 percent / Fetizon's reagent / methanol; H₂O / 8.5 h / Heating

3: 22 percent / triethylamine / methanol / 192 h / Ambient temperature

4: 79 percent / CH₂Cl₂

5: 98 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 2.5 h / 4 °C

With hydrogenchloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; silver carbonate; zinc; In methanol; dichloromethane; water;
DOI:10.1139/v81-062