Trithiocarbonic acid butyl ester 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester

Base Information

• Chemical Name: Trithiocarbonic acid butyl ester 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester
• CAS No.: 78186-86-4
• Molecular Formula: C₁₀H₁₈S₆
• Molecular Weight: 330.649
• Mol file: 78186-86-4.mol

Synonyms:Trithiocarbonic acid butyl ester 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester

Chemical Property of Trithiocarbonic acid butyl ester 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Trithiocarbonic acid butyl ester 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester

There total 1 articles about Trithiocarbonic acid butyl ester 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-<1,2-ethanediylbis(thio)>bis-1,3-dithiolane (33145-02-7) + 1-iodo-butane (542-69-8) → 1,3-dithiolane-2-thione (822-38-8) + dibutyl trithiocarbonate (1608-91-9) + Trithiocarbonic acid butyl ester 2-butylsulfanylthiocarbonylsulfanyl-ethyl ester (78186-90-0) + Trithiocarbonic acid butyl ester 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester (78186-86-4)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -5-(-10) grad C, 30 min, nitrogen, 2.) THF, 1 h at -5-(-10) grad C then 24 h at room temp.;

DOI:10.1016/S0040-4039(01)92515-8

upstream raw materials:

2,2'-<1,2-ethanediylbis(thio)>bis-1,3-dithiolane

1-iodo-butane