({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene

Base Information

Chemical Name:({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene
CAS No.:130625-77-3
Molecular Formula:C₃₆H₆₈OSi₂
Molecular Weight:573.106
Hs Code.:

Synonyms:({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene

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Chemical Property of ({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene

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Technology Process of ({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene

There total 12 articles about ({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130625-75-1
(Z)-3-(Dimethyl-phenyl-silanyl)-hexadec-4-enoic acid benzyl ester

: 130625-77-3
({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: LDA / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) -78 deg C, 1 h

2: LiAlH₄ / diethyl ether / 3 h / 0 °C

3: imidazole / dimethylformamide / 1 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/a804275f

Reference yield:

: 130625-76-2
(Z)-(2R,3S)-3-(Dimethyl-phenyl-silanyl)-2-hexyl-hexadec-4-enoic acid benzyl ester

: 130625-77-3
({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 3 h / 0 °C

2: imidazole / dimethylformamide / 1 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/a804275f

Reference yield:

: 214683-72-4
(Z)-(2R,3S)-3-(Dimethyl-phenyl-silanyl)-2-hexyl-hexadec-4-en-1-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 130625-77-3
({(Z)-(S)-1-[(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-heptyl]-tetradec-2-enyl}-dimethyl-silanyl)-benzene

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 3h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)94466-6