5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-porphine zinc(II)

Base Information

• Chemical Name: 5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-porphine zinc(II)
• CAS No.: 1056647-51-8
• Molecular Formula: C₈₀H₉₆N₈O₄Zn
• Molecular Weight: 1299.08

Synonyms:5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-porphine zinc(II)

Chemical Property of 5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-porphine zinc(II)

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Technology Process of 5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-porphine zinc(II)

There total 2 articles about 5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-porphine zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

5,10,15,20-tetrakis[(3,5,5-trimethylhexanamido)phen-3-yl]-21H,23H-porphine → 5,10,15,20-tetrakis[(3,5,5-trimethylhexanamido)phen-3-yl]-21H,23H-porphine zinc(II) (1056647-51-8)

Guidance literature:

With zinc diacetate; In methanol; chloroform; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1021/ja803434z

Reference yield: 50.0%

5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-21H,23H-porphine + zinc diacetate (557-34-6) → 5,10,15-20-tetrakis(3,5,5-trimethyl-N-phen-3-ylhexanamide)-porphine zinc(II) (1056647-51-8)

Guidance literature:

In methanol; chloroform; a mixture of porphine-compd. and Zn-compd. in CHCl3/CH3OH stirred under N2 at room temp. for 1.5 h; concentrated under reduced pressure, chromy. (deactivated alumina, DCM);

DOI:10.1021/jp803577d

Reference yield:

ethylphosphonic acid diethyl ester (78-38-6) + 5,10,15,20-tetrakis[(3,5,5-trimethylhexanamido)phen-3-yl]-21H,23H-porphine zinc(II) (1056647-51-8) → C6H15O3P*C80H96N8O4Zn

Guidance literature:

In dichloromethane; at 24.84 ℃;

DOI:10.1021/ja803434z

upstream raw materials:

zinc diacetate

Downstream raw materials:

(((CH₃)3CCH₂CH(CH₃)CH₂CONHC₆H₄)4C₂₀H₈N₄)Zn(C₅H₄NCOOC₂H₅)

(((CH₃)3CCH₂CH(CH₃)CH₂CONHC₆H₄)4C₂₀H₈N₄)Zn(C₅H₃N(COOC₂H₅)2)

(((CH₃)3CCH₂CH(CH₃)CH₂CONHC₆H₄)4C₂₀H₈N₄)Zn(C₅H₄NCOOCH₂PO(OC₂H₅)2)

(((CH₃)3CCH₂CH(CH₃)CH₂CONHC₆H₄)4C₂₀H₈N₄)Zn(C₅H₃N(COOCH₂PO(OC₂H₅)2)2)

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