C₃₄H₃₆Br₄N₄O₇

Base Information

Chemical Name:C₃₄H₃₆Br₄N₄O₇
CAS No.:884871-73-2
Molecular Formula:C₃₄H₃₆Br₄N₄O₇
Molecular Weight:932.298
Hs Code.:

C<sub>34</sub>H<sub>36</sub>Br<sub>4</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₄H₃₆Br₄N₄O₇

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Chemical Property of C₃₄H₃₆Br₄N₄O₇

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Technology Process of C₃₄H₃₆Br₄N₄O₇

There total 10 articles about C₃₄H₃₆Br₄N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 884871-61-8
C₃₇H₄₀Br₄N₄O₇

: 884871-73-2
C₃₄H₃₆Br₄N₄O₇

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/jo060084f

Reference yield:

: 884871-43-6
C₁₇H₁₂ClN₃O₅

: 884871-73-2
C₃₄H₃₆Br₄N₄O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: 64 percent / DMAP; triethylamine / CH₂Cl₂ / 0.17 h / 20 °C

2.1: Zn; acetic acid / tetrahydrofuran / 20 °C

3.1: 91 percent / benzyltrimethylammonium tribromide; calcium carbonate / CH₂Cl₂; methanol / 0.5 h / 20 °C

4.1: 88 percent / CuBr₂; t-BuONO / acetonitrile / 1 h / 50 °C

5.1: 90 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1.5 h / 0 °C

6.1: LiHMDS / tetrahydrofuran / 0.58 h / -78 - 20 °C

6.2: 91 percent / tetrahydrofuran / 2 h / -78 °C

7.1: 99 percent / TFA / tetrahydrofuran; H₂O / 20 °C

With dmap; tert.-butylnitrite; ammonium cerium(IV) nitrate; benzyltrimethylammonium tribromide; acetic acid; triethylamine; trifluoroacetic acid; calcium carbonate; copper(ll) bromide; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo060084f

Reference yield:

: 884871-44-7
C₂₂H₂₀ClN₃O₇

: 884871-73-2
C₃₄H₃₆Br₄N₄O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: Zn; acetic acid / tetrahydrofuran / 20 °C

2.1: 91 percent / benzyltrimethylammonium tribromide; calcium carbonate / CH₂Cl₂; methanol / 0.5 h / 20 °C

3.1: 88 percent / CuBr₂; t-BuONO / acetonitrile / 1 h / 50 °C

4.1: 90 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1.5 h / 0 °C

5.1: LiHMDS / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.2: 91 percent / tetrahydrofuran / 2 h / -78 °C

6.1: 99 percent / TFA / tetrahydrofuran; H₂O / 20 °C

With tert.-butylnitrite; ammonium cerium(IV) nitrate; benzyltrimethylammonium tribromide; acetic acid; trifluoroacetic acid; calcium carbonate; copper(ll) bromide; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo060084f