2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester

Base Information

Chemical Name:2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester
CAS No.:616227-08-8
Molecular Formula:C₃₆H₃₄BNO₄
Molecular Weight:555.481
Hs Code.:

Synonyms:2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester

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Chemical Property of 2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester

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Technology Process of 2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester

There total 3 articles about 2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 5570-18-3
2-aminophenylboronic acid

: 130874-89-4
(2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butandiol

: 616227-08-8
2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester

Guidance literature:: In tetrahydrofuran; for 48h; Heating;
DOI:10.1016/S0022-328X(03)00400-5

Reference yield:

: 5570-19-4
2-nitrophenylboronic acid

: 616227-08-8
2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol

2: 76 percent / tetrahydrofuran / 48 h / Heating

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0022-328X(03)00400-5

Reference yield:

: 98-80-6
phenylboronic acid

: 616227-08-8
2-aminophenylboronic acid (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butanediol ester

Guidance literature:: Multi-step reaction with 3 steps

1: HNO₃; Ac₂O; urea

2: H₂ / Pd/C / ethanol

3: 76 percent / tetrahydrofuran / 48 h / Heating

With hydrogen; nitric acid; acetic anhydride; urea; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0022-328X(03)00400-5