Technology Process of N2,N2-bis(2-(diphenylamino)naphthalen-6-yl)-N6,N6-dipheylnaphthalene-2,6-diamine
There total 4 articles about N2,N2-bis(2-(diphenylamino)naphthalen-6-yl)-N6,N6-dipheylnaphthalene-2,6-diamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
PtBu3*HBF4; palladium diacetate;
In
toluene;
at 120 - 121 ℃;
for 18h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / para-xylene / 5 h / 175 - 190 °C / Inert atmosphere; Reflux
1.2: 0.25 h / 55 °C / Reflux; Inert atmosphere
2.1: potassium hydroxide; 1,10-Phenanthroline; copper(l) chloride / toluene / 36 h / 125 °C / Inert atmosphere; Reflux
3.1: sodium t-butanolate / palladium diacetate; PtBu3*HBF4 / toluene / 18 h / 120 - 121 °C / Reflux
With
1,10-Phenanthroline; toluene-4-sulfonic acid; copper(l) chloride; potassium hydroxide; sodium t-butanolate;
PtBu3*HBF4; palladium diacetate;
In
para-xylene; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / para-xylene / 5 h / 175 - 190 °C / Inert atmosphere; Reflux
1.2: 0.25 h / 55 °C / Reflux; Inert atmosphere
2.1: potassium hydroxide; 1,10-Phenanthroline; copper(l) chloride / toluene / 36 h / 125 °C / Inert atmosphere; Reflux
3.1: sodium t-butanolate / palladium diacetate; PtBu3*HBF4 / toluene / 18 h / 120 - 121 °C / Reflux
With
1,10-Phenanthroline; toluene-4-sulfonic acid; copper(l) chloride; potassium hydroxide; sodium t-butanolate;
PtBu3*HBF4; palladium diacetate;
In
para-xylene; toluene;
