tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate

Base Information

Chemical Name:tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate
CAS No.:494795-92-5
Molecular Formula:C₂₂H₃₅N₃O₅
Molecular Weight:421.537
Hs Code.:

Synonyms:tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate

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Chemical Property of tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate

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Technology Process of tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate

There total 1 articles about tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-07-6
N-(methyl)aminoacetaldehyde dimethyl acetal

: 199105-03-8
tert-butyl 4-(2-aminophenyl)piperidine-1-carboxylate

: 494795-92-5
tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate

Guidance literature:: tert-butyl 4-(2-aminophenyl)piperidine-1-carboxylate; With di(succinimido) carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 12h;

N-(methyl)aminoacetaldehyde dimethyl acetal; In DMF (N,N-dimethyl-formamide); dichloromethane; for 12h;

Reference yield:

: 494795-92-5
tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

: 494795-93-6
N-((1R)-1-[(4-Chlorophenyl)methyl]-2-{4-[2-(3-methyl-2-oxo(4-imidazolinyl))-phenyl]piperidyl}-2-oxoethyl)(tert-butoxy)carboxamide

Guidance literature:: tert-Butyl 4-(2-{[(2,2-dimethoxyethyl)methylamino]carbonylamino}-phenyl)piperidinecarboxylate; With trifluoroacetic acid; In water; at 20 ℃; for 2h;

N-Boc-D-(4-Cl)Phe-OH; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

at 20 ℃; for 12h;