Technology Process of C27H29N5O9
There total 11 articles about C27H29N5O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C27H33N5O10;
With
diethylamino-sulfur trifluoride; potassium carbonate;
With
Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene;
DOI:10.1016/j.bmcl.2010.03.086
- Guidance literature:
-
With
Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane;
at -5 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trifluoroacetic acid / dichloromethane / 6.5 h
2.1: hydrogen; trifluoroacetic acid / palladium(II) hydroxide/carbon / tetrahydrofuran; ethanol / 24 h / 20 °C
3.1: 2,6-dimethylpyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 16 h / 20 °C
4.1: diethylamino-sulfur trifluoride / dichloromethane / 4 h / -78 °C
4.2: 1 h / -78 °C
5.1: Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / -5 °C
With
2,6-dimethylpyridine; Bromotrichloromethane; diethylamino-sulfur trifluoride; hydrogen; benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
palladium(II) hydroxide/carbon;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;